2-溴-2-丙烯基乙酸酯合成路线 （共 10 条）
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; pentane T=0°C; 0.5 h;
参考文献
Trost, Barry M.; Yoshida, Jun-ichi; Lautens, Mark
Journal of the American Chemical Society, 1983 , vol. 105, # 13 p. 4494 - 4496
反应条件
1: methylmalonic acid dimethyl ester With sodium hydride in tetrahydrofuran T=20°C; 2: 1-acetoxy-2-bromo-2-propene With tetrakis(triphenylphosphine) palladium(0); sodium methylate in tetrahydrofuran T=20°C; 2.5 h;
参考文献
Journal of Organic Chemistry, , vol. 68, # 10 p. 3918 - 3922
反应条件
1: methylmalonic acid dimethyl ester With sodium hydride in tetrahydrofuran T=20°C; 2: 1-acetoxy-2-bromo-2-propene With tetrakis(triphenylphosphine) palladium(0); phenolated sodium in tetrahydrofuran T=20°C; 16 h;
参考文献
Journal of Organic Chemistry, , vol. 68, # 10 p. 3918 - 3922
参考文献
Helvetica Chimica Acta, , vol. 27, p. 24,29, 40
反应条件
1: methylmalonic acid dimethyl ester; phenol With sodium hydride in tetrahydrofuran
T=20°C; 0.166667 h;
2: 1-acetoxy-2-bromo-2-propene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=20°C; 16 h;
参考文献
Organ, Michael G.; Arvanitis, Elena A.; Hynes, Stephen J.
Journal of Organic Chemistry, 2003 , vol. 68, # 10 p. 3918 - 3922
反应条件
[Pd(dppp)2] in tetrahydrofuran
T=20°C; 5.5 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Organ, Michael G.; Arvanitis, Elena A.; Hynes, Stephen J.
Tetrahedron Letters, 2002 , vol. 43, # 49 p. 8989 - 8992
反应条件
in N,N-dimethyl-formamide
T=40°C;
参考文献
Taylor, Richard E.; Ciavarri, Jeffrey P.
Organic Letters, 1999 , vol. 1, # 3 p. 467 - 469
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in pentane
6 h; Heating;
参考文献
Loepez, Anna; Moreno-Manas, Marcial; Pleixats, Roser; Roglans, Anna
Anales de Quimica, 1997 , vol. 93, # 6 p. 355 - 362
参考文献
Mereshkowski
Justus Liebigs Annalen der Chemie, 1923 , vol. 431, p. 238
参考文献
Mereshkowski
Justus Liebigs Annalen der Chemie, 1923 , vol. 431, p. 238
