Padgett; Degering
Industrial and Engineering Chemistry, 1940 , vol. 32, p. 206
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Frank; Blegen; Deutschman
Journal of Polymer Science, 1948 , vol. 3, p. 58,60
1: n-pentylmagnesium chloride With diethylzinc; (R)-2,2'-dihydroxy-1,1'-binaphthyl in tetrahydrofuran; 1,2-dichloro-ethane
T=-40 - 20°C; 1 h;
2: trifluoro-pyruvic acid ethyl ester in tetrahydrofuran; 1,2-dichloro-ethane
T=-40°C; 24 h; Further stages. Title compound not separated from byproducts.;
参考文献
Gosselin, Francis; Britton, Robert A.; Mowat, Jeffrey; O'Shea, Paul D.; Davies, Ian W.
Synlett, 2007 , # 14 p. 2193 - 2196
Schwartz; Johnson
Journal of the American Chemical Society, 1931 , vol. 53, p. 1065
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Underwood; Gale
Journal of the American Chemical Society, 1934 , vol. 56, p. 2117,2119
