2,4,6-三氯-5-甲基-1,3-苯二酚合成路线 （共 7 条）
参考文献
Stenhouse
Justus Liebigs Annalen der Chemie, 1872 , vol. 163, p. 181
反应条件
sulfuryl dichloride in acetic acid
3 h; Ambient temperature;
参考文献
Henderson, Graeme B.; Hill, Robert A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2595 - 2599
反应条件
phosphorus; hydrogen iodide
参考文献
Stenhouse
Justus Liebigs Annalen der Chemie, 1872 , vol. 163, p. 181
参考文献
Zincke
Chemische Berichte, 1893 , vol. 26, p. 318
反应条件
dipotassium hydrogenphosphate; Fremy’s salt in water
24 h; Ambient temperature;
参考文献
Henderson, Graeme B.; Hill, Robert A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2595 - 2599
反应条件
1: 83 percent / Fremy's salt, K2HPO4 / H2O / 24 h / Ambient temperature
2: 39 percent / NaOH / H2O / 2 h / Heating
3: 1.) H2, 2.) NaOAc / 1.) 10percent Pd-carbon / 1.) ethyl acetate, 1 h, 2.) 100 deg C, 15 min
View Scheme
参考文献
Henderson, Graeme B.; Hill, Robert A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2595 - 2599
反应条件
1: 83 percent / Fremy's salt, K2HPO4 / H2O / 24 h / Ambient temperature
2: 39 percent / NaOH / H2O / 2 h / Heating
View Scheme
参考文献
Henderson, Graeme B.; Hill, Robert A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2595 - 2599
