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1: With trimethylsilyl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; Mukaiyama aldol addition; 2 h; Inert atmosphere; 2: With water; trifluoroacetic acid in ethanol; dichloromethane Inert atmosphere;
参考文献
Downey, C. Wade; Johnson, Miles W.; Lawrence, Daniel H.; Fleisher, Alan S.; Tracy, Kathryn J.
Journal of Organic Chemistry, 2010 , vol. 75, # 15 p. 5351 - 5354