Donaldson, J. D.; Moser, W.; Simpson, W. B.
Journal of the Chemical Society, 1964 , p. 5942 - 5947
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Gmelin Handbook: Sn: MVol.C2, 14.9.2, page 220 - 220
in ethylene glycol dimethyl ether reaction with acetic acid in a suspn. of 1.2-dimethoxyethane under formation of tin(II)-acetate;;
参考文献
Morrison, J. S.; Haendler, H. M.
Journal of Inorganic and Nuclear Chemistry, 1967 , vol. 29, p. 393 - 400
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Gmelin Handbook: Sn: MVol.C1, 3.14.1.1, page 140 - 140
in acetic acid heating Sn in acetic acid under N2 about 80 - 90 h; filtration of soln.; concg. soln.;; drying of residue over KOH; sublimation in vacuum at 150°C;;
参考文献
Donaldson, J. D.; Moser, W.; Simpson, W. B.
Journal of the Chemical Society, 1964 , p. 5942 - 5947
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Gmelin Handbook: Sn: MVol.C2, 14.9.2, page 220 - 220
in tetrahydrofuran sublimation in vacuum (0.05 Torr) at 140°C;;
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Harrison, P. G.; Stobart, S. R.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1973 , p. 940 - 943
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Gmelin Handbook: Sn: MVol.C2, 14.9.2, page 220 - 220
→
反应条件
in acetic acid
参考文献
Donaldson, J. D.; Knifton, J. F.
Journal of the Chemical Society, 1964 , p. 6107 - 6113
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Gmelin Handbook: Sn: MVol.B, 15.1.5.5, page 387 - 391