1-(2,6-二甲基苯基)吡咯烷合成路线 (共 6 条)
反应条件
NiCuFeO(x) in anhydrous xylene
24 h; Inert atmosphereSealed tubeReflux;
参考文献
Cui, Xinjiang; Dai, Xingchao; Deng, Youquan; Shi, Feng
Chemistry - A European Journal, 2013 , vol. 19, # 11 p. 3665 - 3675
反应条件
tris-(dibenzylideneacetone)dipalladium(0); C36H41O2P; sodium t-butanolate in decane; toluene
T=100°C; Buchwald-Hartwig amination; 0.5 h; Inert atmosphere;
参考文献
Doherty, Simon; Knight, Julian G.; McGrady, John P.; Ferguson, Alexandra M.; Ward, Nicholas A. B.; Harrington, Ross W.; Clegg, William
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 1 p. 201 - 211
反应条件
N-ethyl-N,N-diisopropylamine in acetonitrile
T=100°C; 16 h;
参考文献
Camps, P.; Jaime, C.; Molas, J.
Tetrahedron Letters, 1981 , vol. 22, # 26 p. 2487 - 2490
反应条件
aluminum oxide
T=330°C;
参考文献
Walkup, Robert E.; Searles, Scott
Tetrahedron, 1985 , vol. 41, # 1 p. 101 - 106
参考文献
Sommers
Journal of the American Chemical Society, 1956 , vol. 78, p. 2439,2445
反应条件
1.) THF, DMSO, reflux, 2 h, 2.) 200-220 deg C, 1 torr; Yield given. Multistep reaction;
参考文献
Abd-El-Aziz, A.S.; Lee, C. C.; Piorko, A.; Sutherland, R. G.
Journal of Organometallic Chemistry, 1988 , vol. 348, p. 95 - 108