1-(4-硝基苯磺酰基)哌啶合成路线 （共 10 条）
反应条件
pyridine in dichloromethane T=20°C; 2 h;
参考文献
US2006/84802 A1, ;
Page/Page column 30 ;
US 20060084802 A1
反应条件
N-ethyl-N,N-diisopropylamine in acetonitrile T=20°C; Green chemistry;
参考文献
Palakurthy, Nani Babu; Dev, Dharm; Rana, Shubhasmin; Nadimpally, Krishna Chaitanya; Mandal, Bhubaneswar
European Journal of Organic Chemistry, 2013 , # 13 p. 2627 - 2633
反应条件
1-Azidoadamantane in various solvent(s) T=80°C; 6 h;
参考文献
Mukaiyama, Teruaki; Kuroda, Kiichi; Aoki, Hidenori
Chemistry Letters, 2005 , vol. 34, # 12 p. 1644 - 1645
反应条件
in tetrahydrofuran T=20 - 22°C; 0.3 h;
参考文献
Kweon, Deok-Heon; Kim, Ho-Kyun; Kim, Jeum-Jong; Chung, Hyun A.; Woo, Song Lee; Kim, Sung-Kyu; Yoon, Yong-Jin
Journal of Heterocyclic Chemistry, 2002 , vol. 39, # 1 p. 203 - 211
反应条件
1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 0 - 20 °C / |Inert atmosphere 2: N-ethyl-N,N-diisopropylamine / acetonitrile / 20 °C / |Green chemistry View Scheme
参考文献
European Journal of Organic Chemistry, , # 13 p. 2627 - 2633
反应条件
1: DMAP; Et3N / tetrahydrofuran / 20 °C 2: 75 percent / 1-azidoadamantane / various solvent(s) / 6 h / 80 °C View Scheme
参考文献
Chemistry Letters, , vol. 34, # 12 p. 1644 - 1645
反应条件
hydrogenchloride in water; dimethyl sulfoxide T=25°C; Kinetics;
参考文献
Journal of Organic Chemistry, , vol. 69, # 9 p. 3166 - 3172
反应条件
in water; dimethyl sulfoxide T=25°C; Kinetics;
参考文献
Bulletin of the Korean Chemical Society, , vol. 31, # 1 p. 234 - 237
反应条件
N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide Ambient temperature; Yield given;
参考文献
Wuts; Northuis
Tetrahedron Letters, 1998 , vol. 39, # 23 p. 3889 - 3890
反应条件
water; iron; ammonium chloride in ethanol 2 h; Heating / reflux;
参考文献
Pfizer Inc.
Patent: US6407120 B1, 2002 ;
Location in patent: Page column 37 ;
US 6407120 B1
