1,6-内醚-D-半乳糖合成路线 (共 33 条)
反应条件
1: sodium methylate; methanol 2: barium hydroxide; water View Scheme
参考文献
Chemische Berichte, , vol. 88, p. 475,479
反应条件
T=520°C; P=20252 Torr; 1 h; High pressurePyrolysisFlow reactorInert atmosphere; PressureTemperature;
参考文献
Green Chemistry, , vol. 16, # 2 p. 792 - 802
反应条件
T=360°C; P=0.1 Torr; β-D-Galactopyranose;
参考文献
Chemische Berichte, , vol. 62, p. 687,692
反应条件
ammonium hydroxide; osmium(VIII) oxide; 4-methylmorpholine N-oxide 1.) acetone, H2O, RT, 20 h, 2.) CH3OH, RT, overnight; var. 2-O-acyl protected 1,6-anhydro-3,4-dideoxy-β-D-erythro-hex-3-enopyranoses;
参考文献
Heterocycles, , vol. 32, # 11 p. 2225 - 2240
反应条件
enzymes from C. cylindracea; Pancreas different times; Product distribution;
参考文献
Tetrahedron, , vol. 45, # 22 p. 7077 - 7082
参考文献
Chemische Berichte, , vol. 88, p. 475,479
参考文献
Chemische Berichte, , vol. 62, p. 687,692
参考文献
Archives of Biochemistry, , vol. 78, p. 376,377, 379
反应条件
sodium hydride 1) DMF, 2) DMF, 4 h; Yield given. Multistep reaction;
参考文献
Paulsen, Hans; Lockhoff, Oswald
Chemische Berichte, 1981 , vol. 114, # 9 p. 3079 - 3101
反应条件
toluene-4-sulfonic acid in N,N-dimethyl-formamide 1 h; Ambient temperature;
参考文献
Sarbajna, Sumita; Roy, Nirmolendu
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1998 , vol. 37, # 3 p. 252 - 256