1: 3-phenyl-propionyl chloride With triethylamine in dichloromethane
T=20°C; 16 h;
2: furan-2-yl-lithium in tetrahydrofuran
T=0°C; 1 h;
3: With hydrogenchloride in tetrahydrofuran
T=0°C; 0.25 h; Further stages.;
参考文献
Hansen, Anne-Lene L.; Murray, Anthony; Tanner, David
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 24 p. 4497 - 4505
Corey; Ursprung
Journal of the American Chemical Society, 1956 , vol. 78, p. 5041,5047
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Drake; Jacobsen
Journal of the American Chemical Society, 1935 , vol. 57, p. 1570,1572