tetrabutylammomium bromide; sodium carbonate; palladium diacetate in water T=150°C; Suzuki coupling; 0.0833333 h; microwave irradiation;
参考文献
Arvela, Riina K.; Leadbeater, Nicholas E.; Sangi, Michael S.; Williams, Victoria A.; Granados, Patricia; Singer, Robert D.
Journal of Organic Chemistry, 2005 , vol. 70, # 1 p. 161 - 168
tetrabutylammomium bromide; sodium carbonate; palladium contaminants present in sodium carbonate in water T=150°C; Suzuki coupling; 0.0833333 h; microwave irradiation;
参考文献
Arvela, Riina K.; Leadbeater, Nicholas E.; Sangi, Michael S.; Williams, Victoria A.; Granados, Patricia; Singer, Robert D.
Journal of Organic Chemistry, 2005 , vol. 70, # 1 p. 161 - 168
1: (Z)-1,1,1,3,3,3-hexamethyl-2-styryl-2-(trimethylsilyl)trisilane With sodium hydroxide; dihydrogen peroxide in tetrahydrofuran; water T=20°C; 1 h; 2: bromobenzene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; water T=40°C; 12 h;
hydrogen; lt;HIrRu3(CO)13gt; in hexane T=120°C; P=7500.6 Torr; var. cat.: H3IrRu3(CO)12, HIrRu3(CO)11(PhCCPh), HIrRu(CO)10(PhCCPh)(PhCH=CHPh); add. of CO (1 bar); Product distribution;
参考文献
Journal of the Chemical Society - Dalton Transactions, , # 22 p. 3825 - 3831
