ammonium formate; palladium on activated charcoal in water T=20°C; 2.3 h;
参考文献
Nacario, Ruel; Kotakonda, Shailaja; Fouchard, David M. D.; Tillekeratne, L. M. Viranga; Hudson, Richard A.
Organic Letters, 2005 , vol. 7, # 3 p. 471 - 474
1.1: NaH / tetrahydrofuran / 0.67 h / 20 °C
1.2: tetrahydrofuran / 24 h / 20 °C
2.1: NaOMe / methanol / 0.5 h / 20 °C
2.2: H2SO4 / methanol / 2 h / -60 °C
3.1: NaBH4; aq. NaOH / methanol / 20 h / 20 °C
4.1: aq. K2CO3 / 0.25 h / 0 - 4 °C
View Scheme
1.1: NaH / tetrahydrofuran / 0.67 h / 20 °C
1.2: tetrahydrofuran / 24 h / 20 °C
2.1: NaOMe / methanol / 0.5 h / 20 °C
2.2: H2SO4 / methanol / 2 h / -60 °C
View Scheme
参考文献
Janecki, Tomasz; Blaszczyk, Edyta; Studzian, Kazimierz; Janecka, Anna; Krajewska, Urszula; Rozalski, Marek
Journal of Medicinal Chemistry, 2005 , vol. 48, # 10 p. 3516 - 3521
