1: 1-bromo-2-methyl benzene With n-butyllithium in hexane T=-50 - 20°C; 2: dichloro-butyl-phosphine in diethyl ether; hexane 0.5 h; Heating;
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Fey, Natalie; Howell, James A. S.; Lovatt, Jonathan D.; Yates, Paul C.; Cunningham, Desmond; McArdle, Patrick; Gottlieb, Hugo E.; Coles, Simon J.
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Aitken, R. Alan; Cowley, Alan H.; Gabbai, Francois P.; Masamba, Wayiza
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diethyl ether; cadmium (II) chloride
und anschliessend PCl3;
参考文献
Fox
Journal of the American Chemical Society, 1950 , vol. 72, p. 4147,4148
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Weil et al.
Helvetica Chimica Acta, 1953 , vol. 36, p. 1314,1315