3,3'-亚戊烯基-4-丁内酰胺合成路线 （共 23 条）
反应条件
1.1: water; methanol / 80 - 90 °C / |Reflux 2.1: sodium hydrogencarbonate / aq. buffer / 28 h / 25 °C / pH 7.4 - 7.5 / |Enzymatic reaction 2.2: 20 °C 2.3: Raney Nickel / 80 °C / 7500.75 Torr / |Inert atmosphere View Scheme
反应条件
sodium chloride in water-d2 T=80°C; pH=2.24; Kinetics; Further Variations:pH-valuesSolventsTemperatures;
参考文献
Tetrahedron, , vol. 64, # 28 p. 6739 - 6743
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0°C; RefluxInert atmosphere;
参考文献
Wang, Jun; Cady, Sarah D.; Balannik, Victoria; Pinto, Lawrence H.; DeGrado, William F.; Hong, Mei
Journal of the American Chemical Society, 2009 , vol. 131, p. 8066 - 8076
