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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
65119-09-7
合成路线
（共 11 条）
65119-09-7
→
反应条件
103-82-2
苯乙酸
反应条件
KHF2; dihydrogen peroxide in acetic anhydride; N,N-dimethyl-formamide 20 h; Ambient temperature; Yield given;
参考文献
Tamao, Kohei; Kumada, Makoto; Maeda, Kimio
Tetrahedron Letters, 1984 , vol. 25, # 3 p. 321 - 324
588-72-7
+
65119-09-7
→
反应条件
886-65-7
反,反-1,4-二苯基-1,3-丁二烯
+
5808-05-9
反应条件
sodium hydroxide; tetrabutylammomium bromide; 4'-hydroxy-2'-chloropalladioacetophenone oxime dimer in water T=120°C; Hiyama coupling; P=3000.24 - 3750.3 Torr; 0.333333 h; microwave irradiation (40-45 W);
参考文献
Alacid, Emilio; Najera, Carmen
Journal of Organic Chemistry, 2008 , vol. 73, # 6 p. 2315 - 2322
588-72-7
+
65119-09-7
→
反应条件
886-65-7
反,反-1,4-二苯基-1,3-丁二烯
+
5808-05-9
+
35632-82-7
反应条件
sodium hydroxide; 4-hydroacetophenone oxime-derived palladacycle in water T=120°C; Hiyama reaction; 0.333333 h; microwave irradiation;
参考文献
Alacid, Emilio; Najera, Carmen
Journal of Organic Chemistry, 2008 , vol. 73, # 6 p. 2315 - 2322
588-72-7
+
65119-09-7
→
反应条件
886-65-7
反,反-1,4-二苯基-1,3-丁二烯
+
5808-05-9
反应条件
sodium hydroxide; tetrabutylammomium bromide; 4'-hydroxy-2'-chloropalladioacetophenone oxime dimer in water T=120°C; Hiyama coupling; P=3000.24 - 3750.3 Torr; 0.333333 h; microwave irradiation (40-45 W);
参考文献
Alacid, Emilio; Najera, Carmen
Journal of Organic Chemistry, 2008 , vol. 73, # 6 p. 2315 - 2322
588-72-7
+
65119-09-7
→
反应条件
886-65-7
反,反-1,4-二苯基-1,3-丁二烯
+
5808-05-9
+
35632-82-7
反应条件
sodium hydroxide; 4-hydroacetophenone oxime-derived palladacycle in water T=120°C; Hiyama reaction; 0.333333 h; microwave irradiation;
参考文献
Alacid, Emilio; Najera, Carmen
Journal of Organic Chemistry, 2008 , vol. 73, # 6 p. 2315 - 2322
626-55-1
3-溴吡啶
+
65119-09-7
→
反应条件
反应条件
sodium hydroxide; 4-hydroacetophenone oxime-derived palladacycle in water T=120°C; Hiyama reaction; 0.333333 h; microwave irradiation;
参考文献
Alacid, Emilio; Najera, Carmen
Journal of Organic Chemistry, 2008 , vol. 73, # 6 p. 2315 - 2322
90-11-9
1-溴代萘
+
65119-09-7
→
反应条件
28358-65-8
1-(1-苯基乙烯基)-萘
+
2840-88-2
+
2840-87-1
反应条件
sodium hydroxide; 4-hydroxyacetophenone oxime-derived palladacycle in water T=120°C; Hiyama reaction; 0.333333 h; microwave irradiation;
参考文献
Alacid, Emilio; Najera, Carmen
Journal of Organic Chemistry, 2008 , vol. 73, # 6 p. 2315 - 2322
65119-09-7
+
99-91-2
对氯苯乙酮
→
反应条件
3112-03-6
+
20488-43-1
+
87324-13-8
反应条件
sodium hydroxide; 4-hydroacetophenone oxime-derived palladacycle in water T=120°C; Hiyama reaction; 0.5 h; microwave irradiation;
参考文献
Alacid, Emilio; Najera, Carmen
Journal of Organic Chemistry, 2008 , vol. 73, # 6 p. 2315 - 2322
65119-09-7
+
99-90-1
4-溴苯乙酮
→
反应条件
3112-03-6
+
20488-43-1
+
87324-13-8
反应条件
sodium hydroxide; 4-hydroacetophenone oxime-derived palladacycle in water T=120°C; Hiyama reaction; 0.333333 h; microwave irradiation;
参考文献
Alacid, Emilio; Najera, Carmen
Journal of Organic Chemistry, 2008 , vol. 73, # 6 p. 2315 - 2322
104-92-7
4-溴苯甲醚
+
65119-09-7
→
反应条件
4333-75-9
+
1657-53-0
+
1694-19-5
1-甲氧基-4-((E)-苯乙烯基)-苯
反应条件
sodium hydroxide; 4-hydroacetophenone oxime-derived palladacycle in water T=120°C; Hiyama reaction; 0.166667 h; microwave irradiation;
参考文献
Alacid, Emilio; Najera, Carmen
Journal of Organic Chemistry, 2008 , vol. 73, # 6 p. 2315 - 2322
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