2',3',4',5',6'-五氟苯乙酮合成路线 (共 46 条)
反应条件
copper(l) chloride in N,N-dimethyl acetamide T=20°C; 1 h; Inert atmosphereCooling with ice;
参考文献
Russian Journal of Organic Chemistry, , vol. 46, # 3 p. 344 - 351
参考文献
Journal of the American Chemical Society, , vol. 92, p. 6985 - 6987
Ag: MVol.B5, 1.1.3, page 8 - 12
反应条件
aluminium trichloride in carbon disulfide
参考文献
Heterocycles, , vol. 16, # 9 p. 1545 - 1553
反应条件
T=140 - 150°C; 1.66667 h; Title compound not separated from byproducts;
参考文献
Maslennikov, I. G.; Matus, L. I.; Kirichenko, L. N.; Lavrent'ev, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 2 p. 513,467
反应条件
in diethyl ether reaction at 15°C, 15 hours;;
参考文献
Gmelin Handbook: F: PerFHalOrg.4, 2.2.4, page 68 - 115
反应条件
phosphonic acid dimethyl ester in acetonitrile E(a), var. temperatures; KineticsThermodynamic dataRate constant;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 62, # 5.2 p. 1089 - 1091,890 - 891
反应条件
in diethyl ether reaction at 15°C, 15 hours;;
参考文献
Journal of the Chemical Society, , p. 808 - 817
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 39, # 8 p. 1766 - 1773,1730 - 1736
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 39, # 8 p. 1766 - 1773,1730 - 1736
反应条件
1: HNO3 2: aq. NaOH View Scheme
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 39, # 8 p. 1766 - 1773,1730 - 1736