3,6-二氟邻苯二甲酸酐合成路线 （共 15 条）
反应条件
potassium fluoride; NAF T=130 - 270°C; Fluorination; P=20 Torr; Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 19 p. 2755 - 2758
反应条件
1: 80 percent / diethylamine / diethyl ether 2: 1.) n-BuLi / 1.) THF, -78 deg C, 1 h, 2.) -65 deg C, 15 min 3: H2SO4 / H2O / 1 h / Heating 4: 130 °C / 0.05 Torr View Scheme
参考文献
Synthetic Communications, , vol. 20, # 14 p. 2139 - 2146
反应条件
1: 1.) n-BuLi / 1.) THF, -78 deg C, 1 h, 2.) -65 deg C, 15 min 2: H2SO4 / H2O / 1 h / Heating 3: 130 °C / 0.05 Torr View Scheme
参考文献
Synthetic Communications, , vol. 20, # 14 p. 2139 - 2146
反应条件
1: H2SO4 / H2O / 1 h / Heating 2: 130 °C / 0.05 Torr View Scheme
参考文献
Synthetic Communications, , vol. 20, # 14 p. 2139 - 2146
反应条件
T=130°C; P=0.05 Torr; Yield given;
参考文献
Synthetic Communications, , vol. 20, # 14 p. 2139 - 2146
反应条件
1: Zn; NaOH / H2O / 6 h / 70 - 80 °C 2: Zn; NaOH / H2O / 5 h / 95 - 100 °C 3: toluene / Heating 4: KF; NaF / 130 - 270 °C / 20 Torr View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 19 p. 2755 - 2758
反应条件
1: NaOH; H2O / 0.75 h / Heating 2: Zn; NaOH / H2O / 6 h / 70 - 80 °C 3: Zn; NaOH / H2O / 5 h / 95 - 100 °C 4: toluene / Heating 5: KF; NaF / 130 - 270 °C / 20 Torr View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 19 p. 2755 - 2758
反应条件
1: toluene / Heating 2: KF; NaF / 130 - 270 °C / 20 Torr View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 19 p. 2755 - 2758
反应条件
1: Zn; NaOH / H2O / 5 h / 95 - 100 °C 2: toluene / Heating 3: KF; NaF / 130 - 270 °C / 20 Torr View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 19 p. 2755 - 2758
反应条件
1: AlCl3 2: H2SO4 View Scheme
参考文献
Bentov,M. et al.
Bulletin de la Societe Chimique de France, 1970 , p. 1550 - 1552
