2-氯-N,N-二甲基-苯甲酰胺合成路线 （共 20 条）
反应条件
T=170 - 180°C; P=0.7 Torr;
参考文献
Schroth, Werner; Krieg, Reimar; Kluge, Helmut; Gaebler, Michael
Zeitschrift fuer Chemie (Stuttgart, Germany), 1985 , vol. 25, # 11 p. 398 - 399
反应条件
1: oxalyl chloride / CH2Cl2; dimethylformamide / 2 h / Heating
2: pyridine / CH2Cl2 / 20 h
View Scheme
参考文献
Keck, Gary E; McLaws, Mark D; Wager, Travis T
Tetrahedron, 2000 , vol. 56, # 51 p. 9875 - 9883
反应条件
pyridine in dichloromethane
Substitution; 20 h;
参考文献
Keck, Gary E; McLaws, Mark D; Wager, Travis T
Tetrahedron, 2000 , vol. 56, # 51 p. 9875 - 9883
反应条件
copper diacetate; palladium diacetate; copper dichloride
T=120°C; 18 h; Neat (no solvent);
参考文献
Bedford, Robin B.; Engelhart, Jens U.; Haddow, Mairi F.; Mitchell, Charlotte J.; Webster, Ruth L.
Dalton Transactions, 2010 , vol. 39, # 43 p. 10464 - 10472
反应条件
hydrogenchloride
Yield given;
参考文献
Boche, Gernot; Bosold, Ferdinand; Niessner, Manfred
Tetrahedron Letters, 1982 , vol. 23, # 32 p. 3255 - 3256
反应条件
1: 1.) lithium diisopropylamide / 2.) 5 h
2: 2n HCl
View Scheme
参考文献
Boche, Gernot; Bosold, Ferdinand; Niessner, Manfred
Tetrahedron Letters, 1982 , vol. 23, # 32 p. 3255 - 3256
反应条件
2: 1.) lithium diisopropylamide / 2.) 5 h
3: 2n HCl
View Scheme
参考文献
Boche, Gernot; Bosold, Ferdinand; Niessner, Manfred
Tetrahedron Letters, 1982 , vol. 23, # 32 p. 3255 - 3256
反应条件
1: 80 percent / pyridine / 24 h / Ambient temperature
2: 170 - 180 °C / 0.7 Torr
View Scheme
参考文献
Schroth, Werner; Krieg, Reimar; Kluge, Helmut; Gaebler, Michael
Zeitschrift fuer Chemie (Stuttgart, Germany), 1985 , vol. 25, # 11 p. 398 - 399
参考文献
Kirsanow; Solotow
Zhurnal Obshchei Khimii, 1951 , vol. 21, p. 1166,1168; engl. Ausg. S. 1273, 1275
参考文献
Perregaard,J. et al.
Bulletin des Societes Chimiques Belges, 1977 , vol. 86, p. 321 - 328
