(S)-5,5',6,6',7,7',8,8'-八氢-[1,1'-联萘]-2,2'-二酚合成路线 (共 8 条)
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; air; hydrogen in isopropyl alcohol T=20°C; P=38002.6 Torr; 16 h; Molecular sieve;
参考文献
Wang, Da-Wei; Lu, Sheng-Mei; Zhou, Yong-Gui
Tetrahedron Letters, 2009 , vol. 50, # 12 p. 1282 - 1285
反应条件
5-palladium/activated carbon; hydrogen in ethanol; water T=70°C; P=36201.3 Torr; 6 h;
参考文献
Journal of Organic Chemistry, , vol. 74, # 22 p. 8681 - 8689
反应条件
Fmoc-L-Asn(Trt)-L-Asn(Trt)-NH(CH2)6CONH(CH2)3-silica gel in hexane; chloroform
参考文献
Organic Letters, , vol. 7, # 26 p. 5821 - 5823
反应条件
water; cholesterol esterase in diethyl ether T=25°C; catalyst activated by sodium taurocholate; pH = 7.00; rate of hydrolysis (relative to cholesterol acetate); Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 111, # 13 p. 4953 - 4959
反应条件
sodium hydroxide; Raney Ni-Al alloy T=90°C; 6 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 41, # 51 p. 10061 - 10064
反应条件
Fmoc-L-Asn(Trt)-L-Asn(Trt)-NH(CH2)6CONH(CH2)3-silica gel in hexane; chloroform
参考文献
Sun, Ping; Wang, Chunlei; Breitbach, Zachary S.; Zhang, Ying; Armstrong, Daniel W.
Analytical Chemistry, 2009 , vol. 81, # 24 p. 10215 - 10226
反应条件
Fmoc-L-Asn(Trt)-L-Asn(Trt)-NH(CH2)6CONH(CH2)3-silica gel in hexane; chloroform
参考文献
Sun, Ping; Wang, Chunlei; Breitbach, Zachary S.; Zhang, Ying; Armstrong, Daniel W.
Analytical Chemistry, 2009 , vol. 81, # 24 p. 10215 - 10226
反应条件
Fmoc-L-Asn(Trt)-L-Asn(Trt)-NH(CH2)6CONH(CH2)3-silica gel in hexane; chloroform
参考文献
Sun, Ping; Wang, Chunlei; Breitbach, Zachary S.; Zhang, Ying; Armstrong, Daniel W.
Analytical Chemistry, 2009 , vol. 81, # 24 p. 10215 - 10226