2,6-二甲基-1,4-苯二酚合成路线 （共 58 条）
反应条件
1: 100 percent / PdCl2(PhCN)2 / benzene / 2 h / Heating 2: 60 percent / 30percent H2O2, conc. HCl / acetonitrile / 3 h / 50 °C / the excess of H2O2 was removed by catalytic hydrogenation using 10percent Pd-C View Scheme
参考文献
Tetrahedron Letters, , vol. 22, # 25 p. 2337 - 2340
参考文献
Journal of the American Chemical Society, , vol. 72, p. 3252
反应条件
1: copper oxide-chromium oxide; dioxane / 235 °C / 275 Torr / Hydrogenolyse 2: aqueous HBr View Scheme
参考文献
Journal of the American Chemical Society, , vol. 72, p. 3252
反应条件
2: copper oxide-chromium oxide; dioxane / 235 °C / 275 Torr / Hydrogenolyse 3: aqueous HBr View Scheme
参考文献
Journal of the American Chemical Society, , vol. 72, p. 3252
反应条件
1: 76 percent / tetrahydrofuran; diethyl ether / 3 h / -78 - 20 °C 2: 71 percent / PCC; SiO2 / CH2Cl2 / 1 h / 20 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 3, # 19 p. 3479 - 3481
反应条件
1: 81 percent / toluene / 4 h / Heating 2: 76 percent / tetrahydrofuran; diethyl ether / 3 h / -78 - 20 °C 3: 71 percent / PCC; SiO2 / CH2Cl2 / 1 h / 20 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 3, # 19 p. 3479 - 3481
反应条件
cyclohepta-1,3,5-triene in toluene 1.5 h; Heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 58, # 7 p. 2072 - 2077
反应条件
trifluoroacetic acid 1.) CH2Cl2, -20 deg C, 6 h, 2.) CH2Cl2, -20 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 114, # 25 p. 9795 - 9806
参考文献
Justus Liebigs Annalen der Chemie, , vol. 316, p. 279
反应条件
sodium hydroxide; dipotassium peroxodisulfate Erhitzen des mit wss. HCl angesaeuerten Reaktionsgemisches;
参考文献
Journal of the Chemical Society, , p. 1375,1380
Journal of the Chemical Society, , p. 2303,2306
