3-O-苯甲基-alpha-d-吡喃甘露糖合成路线 （共 15 条）
反应条件
in water T=70°C; 12 h; DOWEX 50WX8-400 resin;
参考文献
Xue, Xiaochao; Yin, Zhaojun; Meng, Xiangbao; Li, Zhongjun
Journal of Organic Chemistry, 2013 , vol. 78, # 18 p. 9354 - 9365
反应条件
1: With sodium hydride in N,N-dimethyl-formamide T=0 - 20°C; 3 h; 2: With Amberlite-IR 120(H+) in water 15 h; Heating;
参考文献
Chevalier, Reynald; Colsch, Benoit; Afonso, Carlos; Baumann, Nicole; Tabet, Jean-Claude; Mallet, Jean-Maurice
Tetrahedron, 2006 , vol. 62, # 4 p. 563 - 577
反应条件
Dowex 50 (H(1+)) in water T=70°C; 2 h;
参考文献
Lichtenthaler, Frieder W.; Klaeres, Ulrich; Szurmai, Zoltan; Werner, Bernd
Carbohydrate Research, 1997 , vol. 305, # 2 p. 293 - 303
反应条件
1: 100 percent / NaH; tetrabutylammonium iodide / tetrahydrofuran / 5 h / 20 °C 2: 93 percent / Dowex 50-W (H(+)) / ethanol; H2O / 5 h / Heating View Scheme
参考文献
Carbohydrate Research, , vol. 337, # 10 p. 951 - 954
反应条件
sulfuric acid in methanol 4 h; Heating;
参考文献
Phytochemistry (Elsevier), , vol. 26, # 5 p. 1453 - 1458
反应条件
1: ZnCl2-H3PO4 2: KOH / 2 h / 130 - 150 °C 3: 1M H2SO4 / methanol / 4 h / Heating View Scheme
参考文献
Phytochemistry (Elsevier), , vol. 26, # 5 p. 1453 - 1458
反应条件
1: KOH / 2 h / 130 - 150 °C 2: 1M H2SO4 / methanol / 4 h / Heating View Scheme
参考文献
Phytochemistry (Elsevier), , vol. 26, # 5 p. 1453 - 1458
反应条件
1: KOH / 2 h / 130 - 150 °C 2: 1M H2SO4 / methanol / 4 h / Heating View Scheme
参考文献
Phytochemistry (Elsevier), , vol. 26, # 5 p. 1453 - 1458
反应条件
1: 100 percent / NaH; tetrabutylammonium iodide / tetrahydrofuran / 5 h / 20 °C 2: 93 percent / Dowex 50-W (H(+)) / ethanol; H2O / 5 h / Heating View Scheme
参考文献
Carbohydrate Research, , vol. 337, # 10 p. 951 - 954
反应条件
sodium hydride 1.) NN-dimethylformamide, overnight, 2.) Dowex 50 resin (H+), aq. ethanol, 90 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1971 - 1977
