in ethanol EtOH soln. of ligand added dropwise to warm EtOH soln. of metal chloride, mixt. stirred for 1 h, cooled to room temp.; filtered off, washed (EtOH), dried (vac.);
in not given direct mixing of CuCl2 and the ligand in the required proportion;
参考文献
Mikhailov, O. V.; Polovnyak, V. K.
Inorganic Materials (Transl. of Neorg. Mater.), 1991 , vol. 27, p. 288 - 292
Izvestiya Akademii Nauk SSSR, Neorganicheskie Materialy, 1991 , vol. 27, p. 370 - 375
