二苯基碘三氟甲烷磺酸盐合成路线 (共 201 条)
反应条件
N,N,N',N,-tetramethylethylenediamine; sodium hydrogencarbonate T=80°C; 10 h; under air;
参考文献
Journal of Organic Chemistry, , vol. 77, # 1 p. 766 - 771
反应条件
palladium diacetate in N,N-dimethyl-formamide P=760 Torr; 0.5 h; Ambient temperature;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 5 p. 841 - 842
反应条件
copper(II) bis(trifluoromethanesulfonate); sodium salt of phosphorous acid in toluene T=100°C; 15 h; Inert atmosphere; chemoselective reaction;
参考文献
Kuriyama, Masami; Hamaguchi, Norihisa; Onomura, Osamu
Chemistry - A European Journal, 2012 , vol. 18, # 6 p. 1591 - 1594
反应条件
lithium hexamethyldisilazane in tetrahydrofuran; N,N-dimethyl-formamide T=-78 - -45°C;
参考文献
Aggarwal, Varinder K.; Olofsson, Berit
Angewandte Chemie - International Edition, 2005 , vol. 44, # 34 p. 5516 - 5519
反应条件
lithium diisopropyl amide 1.) THF, -78 deg C, 1 h; 2.) -35 deg C, 15 min, -78 deg C; 3.) -78 deg C, 15 min, r.t., 1 h; Product distribution;
参考文献
Ryan, John H.; Stang, Peter J.
Tetrahedron Letters, 1997 , vol. 38, # 28 p. 5061 - 5064
反应条件
palladium diacetate in N,N-dimethyl-formamide P=760 Torr; 0.5 h; Ambient temperature;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 5 p. 841 - 842
反应条件
1: 62 percent / Pd(OAc)2 / dimethylformamide / 0.5 h / 760 Torr / Ambient temperature 2: Pd(OAc)2 / dimethylformamide / 0.5 h / 760 Torr / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 5 p. 841 - 842
反应条件
xanthone powder in acetonitrile Irradiation; Product distribution;
参考文献
Dektar, John L.; Hacker, Nigel P.
Journal of Organic Chemistry, 1990 , vol. 55, # 2 p. 639 - 647
反应条件
in acetone Irradiation; Quantum yieldProduct distributionMechanism;
参考文献
Dektar, John L.; Hacker, Nigel P.
Journal of Organic Chemistry, 1991 , vol. 56, # 5 p. 1838 - 1844
反应条件
in acetonitrile Irradiation0.02m chlorobenzene; Product distribution;
参考文献
Dektar, John L.; Hacker, Nigel P.
Journal of Organic Chemistry, 1990 , vol. 55, # 2 p. 639 - 647