二苯基碘三氟甲烷磺酸盐合成路线 (共 201 条)
反应条件
lithium diisopropyl amide 1.) THF, -78 deg C, 1 h; 2.) -35 deg C, 15 min, -78 deg C; 3.) -78 deg C, 15 min, r.t., 1 h; Yield given. Multistep reaction;
参考文献
Ryan, John H.; Stang, Peter J.
Tetrahedron Letters, 1997 , vol. 38, # 28 p. 5061 - 5064
反应条件
palladous nitrate; Ir(ppy)2(dtbbpy)PF6 in methanol T=20°C; 15 h; UV-irradiationInert atmosphere;
参考文献
Neufeldt, Sharon R.; Sanford, Melanie S.
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 18 p. 3517 - 3522
反应条件
potassium tert-butylate in N,N-dimethyl-formamide 1 h; Inert atmosphereReflux;
参考文献
Jalalian, Nazli; Petersen, Tue B.; Olofsson, Berit
Chemistry--A European Journal, 2012 , vol. 18, # 44 p. 14140 - 14149,10
反应条件
triethylamine; copper(l) chloride in dichloromethane T=20°C; 0.166667 h; Schlenk technique;
参考文献
Journal of Organic Chemistry, , vol. 78, # 16 p. 8176 - 8183
反应条件
triethylamine; copper(l) chloride in dichloromethane T=20°C; 0.166667 h; Schlenk technique;
参考文献
Xu, Jian; Zhang, Pengbo; Gao, Yuzhen; Chen, Yiyin; Tang, Guo; Zhao, Yufen
Journal of Organic Chemistry, 2013 , vol. 78, # 16 p. 8176 - 8183
反应条件
in N,N-dimethyl-formamide T=90°C; 24 h; Inert atmosphereSchlenk technique;
参考文献
Umierski, Natalie; Manolikakes, Georg
Organic Letters, 2013 , vol. 15, # 19 p. 4972 - 4975
反应条件
in N,N-dimethyl-formamide T=90°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Umierski, Natalie; Manolikakes, Georg
Organic Letters, 2013 , vol. 15, # 1 p. 188 - 191
反应条件
water; oxygen; copper diacetate in dichloromethane T=80°C; 16 h; regioselective reaction;
参考文献
Xu, Ze-Feng; Cai, Chen-Xin; Liu, Jin-Tao
Organic Letters, 2013 , vol. 15, # 9 p. 2096 - 2099
反应条件
triethylamine; copper(l) chloride in dichloromethane T=20°C; 0.166667 h; Schlenk technique;
参考文献
Xu, Jian; Zhang, Pengbo; Gao, Yuzhen; Chen, Yiyin; Tang, Guo; Zhao, Yufen
Journal of Organic Chemistry, 2013 , vol. 78, # 16 p. 8176 - 8183
反应条件
2,6-di-tert-butyl-pyridine; copper(II) bis(trifluoromethanesulfonate) in dichloromethane T=20°C; 39 h;
参考文献
Phipps, Robert J.; Grimster, Neil P.; Gaunt, Matthew J.
Journal of the American Chemical Society, 2008 , vol. 130, # 26 p. 8172 - 8174