二苯基碘三氟甲烷磺酸盐合成路线 (共 201 条)
反应条件
trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); trifluoroacetic acid T=100°C; 24 h; Overall yield = 63 percent; Overall yield = 33.1 mg;
参考文献
Storr, Thomas E.; Greaney, Michael F.
Organic Letters, 2013 , vol. 15, # 6 p. 1410 - 1413
反应条件
sodium hydroxide T=80°C; 10 h; under air;
参考文献
Wen, Jun; Zhang, Ruo-Yi; Chen, Shan-Yong; Zhang, Ji; Yu, Xiao-Qi
Journal of Organic Chemistry, 2012 , vol. 77, # 1 p. 766 - 771
反应条件
sodium hydroxide T=80°C; 10 h; under air; regioselective reaction;
参考文献
Wen, Jun; Zhang, Ruo-Yi; Chen, Shan-Yong; Zhang, Ji; Yu, Xiao-Qi
Journal of Organic Chemistry, 2012 , vol. 77, # 1 p. 766 - 771
反应条件
trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); trifluoroacetic acid T=100°C; 24 h; Overall yield = 67 percent; Overall yield = 28 mg;
参考文献
Storr, Thomas E.; Greaney, Michael F.
Organic Letters, 2013 , vol. 15, # 6 p. 1410 - 1413
反应条件
trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); trifluoroacetic acid T=100°C; 24 h; Overall yield = 47 percent;
参考文献
Organic Letters, , vol. 15, # 6 p. 1410 - 1413
反应条件
1: indole-2,3-dione With sodium hydride in N,N-dimethyl-formamide; mineral oil T=25°C; Inert atmosphere; 2: Diphenyliodonium triflate in N,N-dimethyl-formamide; mineral oil T=40°C; 1 h; Inert atmosphere;
参考文献
Bergman, Jan; Stensland, Birgitta
Journal of Heterocyclic Chemistry, 2014 , vol. 51, # 1 p. 1 - 10
反应条件
potassium thiocyanate in neat (no solvent) T=120°C; 0.25 h; Microwave irradiation; regioselective reaction;
参考文献
Vaddula, Buchi Reddy; Varma, Rajender S.; Leazer, John
European Journal of Organic Chemistry, 2012 , # 35 p. 6852 - 6855
反应条件
palladium(II)-supported on dopamine-functionalized Fe3O4 nanoparticles in polyethylene glycol-400; water T=20°C; Heck type arylation reaction; 12 h;
参考文献
Green Chemistry, , vol. 14, # 8 p. 2133 - 2136
反应条件
potassium tert-butylate in toluene 1 h; Inert atmosphereReflux;
参考文献
Petersen, Tue B.; Khan, Rehan; Olofsson, Berit
Organic Letters, 2011 , vol. 13, # 13 p. 3462 - 3465
反应条件
potassium fluoride; 4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]hexacosane in acetonitrile-D3 T=80°C; 1 h; Product distribution / selectivity;
参考文献
GE HEALTHCARE LIMITED
Patent: WO2005/61415 A1, 2005 ;
Location in patent: Page/Page column 11-12 ;