二苯基碘三氟甲烷磺酸盐合成路线 (共 201 条)
反应条件
potassium fluoride; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; 4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]hexacosane in acetonitrile-D3 Product distribution / selectivity;
参考文献
GE HEALTHCARE LIMITED
Patent: WO2005/61415 A1, 2005 ;
Location in patent: Page/Page column 13 ;
反应条件
trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); trifluoroacetic acid T=100°C; 24 h; Overall yield = 47 percent;
参考文献
Organic Letters, , vol. 15, # 6 p. 1410 - 1413
反应条件
palladium diacetate in N,N-dimethyl-formamide T=130°C; 0.0333333 h; Schlenk techniqueMicrowave irradiation; regioselective reaction;
参考文献
Li, Jian; Liu, Li; Ding, Dong; Sun, Jiang-Tao
Letters in Organic Chemistry, 2013 , vol. 10, # 1 p. 42 - 46
反应条件
trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); trifluoroacetic acid T=100°C; 24 h; Overall yield = 67 percent; Overall yield = 28 mg;
参考文献
Storr, Thomas E.; Greaney, Michael F.
Organic Letters, 2013 , vol. 15, # 6 p. 1410 - 1413
反应条件
palladium(II)-supported on dopamine-functionalized Fe3O4 nanoparticles in polyethylene glycol-400; water T=20°C; Heck type arylation reaction; 12 h;
参考文献
Vaddula, Buchi Reddy; Saha, Amit; Leazer, John; Varma, Rajender S.
Green Chemistry, 2012 , vol. 14, # 8 p. 2133 - 2136
反应条件
palladium diacetate in tetrahydrofuran T=60°C; 24 h;
参考文献
Research on Chemical Intermediates, , vol. 38, # 7 p. 1335 - 1340
反应条件
2,6-di-tert-butyl-pyridine; copper(II) bis(trifluoromethanesulfonate) in dichloromethane T=20°C; 26 h;
参考文献
Phipps, Robert J.; Grimster, Neil P.; Gaunt, Matthew J.
Journal of the American Chemical Society, 2008 , vol. 130, # 26 p. 8172 - 8174
反应条件
palladium diacetate in tetrahydrofuran T=20°C; 24 h;
参考文献
Yang, Qi; Chang, Jiao; Wu, Qun; Zhang, Bianxiang
Research on Chemical Intermediates, 2012 , vol. 38, # 7 p. 1335 - 1340
反应条件
PEG-400 T=50°C; 0.166667 h; Microwave irradiationSealed tube; SolventTime;
参考文献
Kumar, Dalip; Arun; Pilania, Meenakshi; Shekar, K.P. Chandra
Synlett, 2013 , vol. 24, # 7 art. no. ST-2013-D0144-L, p. 831 - 836
反应条件
1: 4-methyl-N-morpholin-4-ylbenzenesulfonamide With benzyl bromide; potassium carbonate in 1,4-dioxane T=50°C; 1 h; 2: Diphenyliodonium triflate T=100°C; 15 h;
参考文献
Richards-Taylor, Charlotte S.; Blakemore, David C.; Willis, Michael C.
Chemical Science, 2013 , vol. 5, # 1 p. 222 - 228