potassium tert-butylate in tetrahydrofuran
T=20°C; 2 h;
参考文献
Barlow, Stephen; Risko, Chad; Chung, Sung-Jae; Tucker, Neil M.; Coropceanu, Veaceslav; Jones, Simon C.; Levi, Zerubba; Bredas, Jean-Luc; Marder, Seth R.
Journal of the American Chemical Society, 2005 , vol. 127, # 48 p. 16900 - 16911
Gao, Lei; Niedzwiecki, Daniel S.; Deligonul, Nihal; Zeller, Matthias; Hunter, Allen D.; Gray, Thomas G.
Chemistry - A European Journal, 2012 , vol. 18, # 20 p. 6316 - 6327
1: benzene / 18 h / Reflux
2: n-butyllithium / tetrahydrofuran / -78 °C
View Scheme
参考文献
Gao, Lei; Niedzwiecki, Daniel S.; Deligonul, Nihal; Zeller, Matthias; Hunter, Allen D.; Gray, Thomas G.
Chemistry - A European Journal, 2012 , vol. 18, # 20 p. 6316 - 6327
1: With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 1 h;
2: With phosphorus trichoride in tetrahydrofuran; hexane
T=-78 - 20°C; Further stages.;
参考文献
Smith, Rhett C.; Protasiewicz, John D.
Dalton Transactions, 2003 , # 24 p. 4738 - 4741
