tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran (Ar), stirred for 48 h at room temp.; total adduct yield 76percent; removed solvent; GLC, NMR;
参考文献
Mitchell, Terence N.; Schneider, Ulrich
Journal of Organometallic Chemistry, 1991 , vol. 405, # 2 p. 195 - 199
tetrakis(triphenylphosphine) palladium(0) in toluene byproducts: (((CH3)3C)(CH3)2Si)2; mixt. of 2 equiv of isonitrile and 5 equiv of organosilylstannane and 0.06 equiv of Pd-complex was heated in toluene at 60°C for 3 h under Ar; distd.; elem. anal.;;
参考文献
Ito, Yoshihiko; Bando, Takashi; Matsuura, Takaharu; Ishikawa, Mitsuo
Journal of the Chemical Society, Chemical Communications, 1986 , # 12 p. 980 - 981
in diethyl ether byproducts: i-Pr2NH; Schlenk tube charged with Me3SnN-i-Pr2 (1.25 mmol) and TMTH (1. 25 mmol) in Et2O under Ar, stirred for 2 h at room temp.; GC analysis;
参考文献
Reimann, Werner; Kuivila, Henry G.; Farah, Dan; Apoussidis, Theodorus
Organometallics, 1987 , vol. 6, p. 557 - 565
tert-butylamine in tetrahydrofuran LiSnMe3 added to mixt. of (1-naphthyl)SnEt3 and t-butylamine in THF, stirred at 50°C for 30 min, hydrolysis with water; extd. with ether, org. layer dried over Na2SO4; yields of products determined by GLC;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 9 p. 3299 - 3306
