4-甲氧基三氟甲烷磺酸苯酯合成路线 （共 120 条）
反应条件
2,6-dimethylpyridine in dichloromethane T=20°C; 16 h;
参考文献
Uchiyama, Masanobu; Kobayashi, Yuri; Furuyama, Taniyuki; Nakamura, Shinji; Kajihara, Yumiko; Miyoshi, Tomoko; Sakamoto, Takao; Kondo, Yoshinori; Morokuma, Keiji
Journal of the American Chemical Society, 2008 , vol. 130, # 2 p. 472 - 480
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; Acylation; 8 h;
参考文献
Wentworth; Wentworth Jr.; Mansoor; Janda
Organic letters, 2000 , vol. 2, # 4 p. 477 - 480
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; Acylation; 8 h;
参考文献
Wentworth; Wentworth Jr.; Mansoor; Janda
Organic letters, 2000 , vol. 2, # 4 p. 477 - 480
反应条件
7-methyl-1,5,7-triazabicyclo[4.4.0]dec-5-ene on polystyrene.HL in acetonitrile T=80°C; Esterification;
参考文献
Boisnard, Sabine; Chastanet, Jaqueline; Zhu, Jieping
Tetrahedron Letters, 1999 , vol. 40, # 42 p. 7469 - 7472
反应条件
pyridine in dichloromethane T=20°C; 2 h;
参考文献
Journal of the American Chemical Society, , vol. 123, # 36 p. 8864 - 8865
反应条件
1: n-butyllithium With zinc(II) chloride in tetrahydrofuran; hexane T=0°C; transmetallation; 0.25 h; 2: 3-iodo-4-methoxyphenyl trifluoromethanesulfonate in tetrahydrofuran; hexane T=20°C; Metallation; alkylation; 8 h; 3: With hydrogenchloride in tetrahydrofuran; hexane Hydrolysis;
参考文献
Harada, Toshiro; Chiba, Minako; Oku, Akira
Journal of Organic Chemistry, 1999 , vol. 64, # 22 p. 8210 - 8213
反应条件
Pd(CH2SiMe3)2(cod); t-Bu Brett Phos; cesium fluoride in toluene T=130°C; 12 h;
参考文献
Maimone, Thomas J.; Milner, Phillip J.; Kinzel, Tom; Zhang, Yong; Takase, Michael K.; Buchwald, Stephen L.
Journal of the American Chemical Society, 2011 , vol. 133, # 45 p. 18106 - 18109
反应条件
in toluene T=120°C; 3 h; Inert atmosphere;
参考文献
Maimone, Thomas J.; Milner, Phillip J.; Kinzel, Tom; Zhang, Yong; Takase, Michael K.; Buchwald, Stephen L.
Journal of the American Chemical Society, 2011 , vol. 133, # 45 p. 18106 - 18109
反应条件
NiII chloride hexahydrate; potassium bromide T=185 - 190°C; Arbuzov reaction; 20 h; Inert atmosphere;
参考文献
Yang, Guoqiang; Shen, Chaoren; Zhang, Liang; Zhang, Wanbin
Tetrahedron Letters, 2011 , vol. 52, # 39 p. 5032 - 5035
反应条件
pyridine; 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate T=150°C; 0.333333 h; microwave irradiation;
参考文献
Lesma, Giordano; Sacchetti, Alessandro; Silvani, Alessandra
Synthesis, 2006 , # 4 p. 594 - 596
