4-甲氧基三氟甲烷磺酸苯酯合成路线 （共 120 条）
反应条件
tetra-n-butylammonium tetrafluoroborate; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide T=90°C; electrochemical reaction;
参考文献
European Journal of Organic Chemistry, , # 9 p. 1811 - 1821
反应条件
biphenyl-2-yl-di-tert-butyl-phosphane; sodium t-butanolate; tris(dibenzylideneacetone)dipalladium (0) in toluene T=20°C; Arylation; 48 h;
参考文献
Wolfe, John P.; Tomori, Hiroshi; Sadighi, Joseph P.; Yin, Jingjun; Buchwald, Stephen L.
Journal of Organic Chemistry, 2000 , vol. 65, # 4 p. 1158 - 1174
反应条件
potassium acetate; bis(dibenzylideneacetone)-palladium(0); tri-cyclo-hexyl-phosphine in 1,4-dioxane T=80°C; 2 h;
参考文献
Ishiyama, Tatsuo; Ishida, Kousaku; Miyaura, Norio
Tetrahedron, 2001 , vol. 57, # 49 p. 9813 - 9816
反应条件
triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane T=80°C; borylation; 4 h;
参考文献
Journal of Organic Chemistry, , vol. 65, # 1 p. 164 - 168
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane T=80°C; 13 h;
参考文献
Ishiyama, Tatsuo; Itoh, Yoshiya; Kitano, Takahiro; Miyaura, Norio
Tetrahedron Letters, 1997 , vol. 38, # 19 p. 3447 - 3450
反应条件
Pd(CH2SiMe3)2(cod); t-Bu Brett Phos; cesium fluoride in toluene T=130°C; 12 h;
参考文献
Maimone, Thomas J.; Milner, Phillip J.; Kinzel, Tom; Zhang, Yong; Takase, Michael K.; Buchwald, Stephen L.
Journal of the American Chemical Society, 2011 , vol. 133, # 45 p. 18106 - 18109
反应条件
triethylamine; acetone in 2,2,2-trifluoroethanol 60 h; Irradiation;
参考文献
Protti, Stefano; Fagnoni, Maurizio; Albini, Angelo
Angewandte Chemie - International Edition, 2005 , vol. 44, # 35 p. 5675 - 5678
反应条件
1: 4-methoxyphenyl triflate With dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; anhydrous lithium acetate; palladium diacetate in tert-butyl methyl ether T=25°C; 0.166667 h; Inert atmosphereGlovebox; 2: γ-butyrolactone trimethylsilyl enol ether in tert-butyl methyl ether T=25°C; 2 h; Inert atmosphereGlovebox; enantioselective reaction;
参考文献
Huang, Zhiyan; Chen, Zuliang; Lim, Li Hui; Quang, Gia Chuong Phan; Hirao, Hajime; Zhou, Jianrong
Angewandte Chemie - International Edition, 2013 , vol. 52, # 22 p. 5807 - 5812
Angew. Chem., 2013 , vol. 125, # 22 p. 5919 - 5924
反应条件
in toluene T=120°C; 3 h; Inert atmosphere;
参考文献
Maimone, Thomas J.; Milner, Phillip J.; Kinzel, Tom; Zhang, Yong; Takase, Michael K.; Buchwald, Stephen L.
Journal of the American Chemical Society, 2011 , vol. 133, # 45 p. 18106 - 18109
反应条件
potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in dimethyl sulfoxide T=80°C; 3 h;
参考文献
Synthesis, , # 4 art. no. M05304SS, p. 547 - 550
