4-甲氧基三氟甲烷磺酸苯酯合成路线 （共 120 条）
反应条件
1,3-bis-(diphenylphosphino)propane; triethylamine; palladium diacetate in dimethyl sulfoxide T=70°C; 1 h;
参考文献
Dolle, Roland E.; Schmidt, Stanley J.; Kruse, Lawrence I.
Journal of the Chemical Society, Chemical Communications, 1987 , # 12 p. 904 - 905
反应条件
triethylamine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in propan-1-ol Suzuki cross-coupling reaction; 3 h; Heating;
参考文献
Molander, Gary A.; Rivero, Marta Rodriguez
Organic Letters, 2002 , vol. 4, # 1 p. 107 - 109
反应条件
pyridine; 2,6-di-tert-butyl-4-methyl-phenol; pyridine hydrogenfluoride; lithium chloride; tetrakis(triphenylphosphine) palladium(0) 1.) 1,4-dioxane, reflux, 6.5 h, 2.) THF, 23 deg C, 16 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Echavarren,A.M.; Stille,J.K.
Journal of the American Chemical Society, 1987 , vol. 109, p. 5478
反应条件
potassium phosphate; 2-(dicyclohexylphosphino)biphenyl based D-gluconamide; palladium diacetate in water T=80°C; 16 h;
参考文献
Tetrahedron, , vol. 58, # 29 p. 5779 - 5787
反应条件
caesium carbonate; tri-cyclo-hexyl-phosphine; palladium diacetate in tetrahydrofuran Suzuki-Miyaura reaction; 21 h; Heating;
参考文献
Synlett, , # 11 art. no. Y00205ST, p. 1763 - 1766
反应条件
potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0) in tert-butyl alcohol T=110°C;
参考文献
Ikawa, Takashi; Barder, Timothy E.; Biscoe, Mark R.; Buchwald, Stephen L.
Journal of the American Chemical Society, 2007 , vol. 129, # 43 p. 13001 - 13007
反应条件
oxygen in methanol 6 h; Photolysis; MechanismQuantum yield; Reagent/catalyst;
参考文献
Terpolilli, Marco; Merli, Daniele; Protti, Stefano; Dichiarante, Valentina; Fagnoni, Maurizio; Albini, Angelo
Photochemical and Photobiological Sciences, 2011 , vol. 10, # 1 p. 123 - 127
反应条件
tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl T=50°C; 4 h; Inert atmosphereMolecular sieveNeat (no solvent);
参考文献
Walvoord, Ryan R.; Berritt, Simon; Kozlowski, Marisa C.
Organic Letters, 2012 , vol. 14, # 16 p. 4086 - 4089
反应条件
1,3-bis-(diphenylphosphino)propane; 1,1,1,3,3,3-hexamethyl-disilazane; palladium dichloride in N,N-dimethyl-formamide T=100°C; 2.5 h;
参考文献
Morera, Enrico; Ortar, Giorgio
Tetrahedron Letters, 1998 , vol. 39, # 18 p. 2835 - 2838
反应条件
tetra-(n-butyl)ammonium iodide; triethylamine; [Rhacetylacetonate(1,5-cyclooctadiene)] in N,N-dimethyl-formamide T=100°C; 16 h;
参考文献
Murata, Miki; Yamasaki, Hiyoruki; Ueta, Tsukasa; Nagata, Masayuki; Ishikura, Masanori; Watanabe, Shinji; Masuda, Yuzuru
Tetrahedron, 2007 , vol. 63, # 19 p. 4087 - 4094
