4-甲氧基三氟甲烷磺酸苯酯合成路线 （共 120 条）
反应条件
tetrabutyl ammonium fluoride; palladium diacetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tert-butyl alcohol T=60°C; Hiyama cross-coupling reaction; Inert atmosphere;
参考文献
Molander, Gary A.; Iannazzo, Laura
Journal of Organic Chemistry, 2011 , vol. 76, # 21 p. 9182 - 9187
反应条件
palladium diacetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in toluene T=120°C; 24 h; Sealed tubeInert atmosphere;
参考文献
Zhou, Chao; Liu, Qingjiang; Li, Yaming; Zhang, Rong; Fu, Xinmei; Duan, Chunying
Journal of Organic Chemistry, 2012 , vol. 77, # 22 p. 10468 - 10472
反应条件
1,2-dimethoxy-benzene; Pd(F6-acac)2; 1,3-bis-(diphenylphosphino)propane; lithium carbonate T=120°C; Heck Reaction; 48 h; Inert atmosphere;
参考文献
Wu, Xiaojin; Lu, Yunpeng; Hirao, Hajime; Zhou, Jianrong
Chemistry - A European Journal, 2013 , vol. 19, # 19 p. 6014 - 6020
反应条件
potassium fluoride; tris-(dibenzylideneacetone)dipalladium(0); t-Bu Brett Phos; potassium bromide in 1,4-dioxane T=130°C; 16 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 13, # 18 p. 4974 - 4976
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate in toluene T=85°C; 8 h;
参考文献
Louie, Janis; Driver, Michael S.; Hamann, Blake C.; Hartwig, John F.
Journal of Organic Chemistry, 1997 , vol. 62, # 5 p. 1268 - 1273
反应条件
2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl; tris(dibenzylideneacetone)dipalladium (0) in tetrahydrofuran 4 h; Heating;
参考文献
Cooper, Thea; Novak, Andrew; Humphreys, Luke D.; Walker, Matthew D.; Woodward, Simon
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 6 p. 686 - 690
反应条件
ammonium hydroxide; 2,6-di-tert-butyl-4-methyl-phenol; lithium chloride; tetrakis(triphenylphosphine) palladium(0) 1.) 1,4-dioxane, reflux, 85 deg C, 13 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Echavarren,A.M.; Stille,J.K.
Journal of the American Chemical Society, 1987 , vol. 109, p. 5478
反应条件
tris-(dibenzylideneacetone)dipalladium(0); 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tetrahydrofuran T=90°C; 4 h; Inert atmosphere;
参考文献
Vinogradov, Andrej; Woodward, Simon; Rageot, Denise; Pfaltz, Andreas
Organic Syntheses, 2010 , vol. 87, p. 104 - 114
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium acetate in tetrahydrofuran Suzuki-Miyaura cross-coupling; RefluxInert atmosphere;
参考文献
Wang, Bing; Sun, Hui-Xia; Sun, Zhi-Hua
European Journal of Organic Chemistry, 2009 , # 22 p. 3688 - 3692
反应条件
oxygen in methanol 6 h; Photolysis; MechanismQuantum yield; Reagent/catalyst;
参考文献
Terpolilli, Marco; Merli, Daniele; Protti, Stefano; Dichiarante, Valentina; Fagnoni, Maurizio; Albini, Angelo
Photochemical and Photobiological Sciences, 2011 , vol. 10, # 1 p. 123 - 127
