(2-溴-1-氯-乙基)苯合成路线 (共 10 条)
反应条件
tri-N-methyl-anilinium; dichloro bromate(I) in chloroform
T=15°C;
参考文献
Negoro; Ikeda
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 8 p. 2111 - 2115
反应条件
thionyl chloride
T=65°C;
参考文献
Braddock, D. Christopher; Hermitage, Stephen A.; Kwok, Lilian; Pouwer, Rebecca; Redmond, Joanna M.; White, Andrew J. P.
Chemical Communications, 2009 , # 9 p. 1082 - 1084
反应条件
sodium hypochlorite; potassium bromide in phosphate buffer; acetonitrile
T=40°C; pH=10.4; 1 h;
参考文献
Klawonn, Markus; Bhor, Santosh; Mehltretter, Gerald; Doebler, Christian; Fischer, Christine; Beller, Matthias
Advanced Synthesis and Catalysis, 2003 , vol. 345, # 3 p. 389 - 392
反应条件
tri-hexyltetradecylphosphonium chloride; trihexyltetradecylphosphonium dibromochloride in chloroform-d1
T=20°C; 1 h; DarknessIonic liquid; regioselective reaction;
参考文献
Cristiano, Rodrigo; Ma, Kefeng; Pottanat, George; Weiss, Richard G.
Journal of Organic Chemistry, 2009 , vol. 74, # 23 p. 9027 - 9033
反应条件
n-Bu4NBrCl2 in acetic acid
T=20°C; Yield given. Yields of byproduct given;
参考文献
Negoro, Takeshi; Ikeda, Yoshitsugu
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 3519 - 3522
参考文献
Buckles; Long
Journal of the American Chemical Society, 1951 , vol. 73, p. 998
反应条件
n-Bu4NBrCl2
T=20°C; Yield given. Yields of byproduct given;
参考文献
Negoro, Takeshi; Ikeda, Yoshitsugu
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 3519 - 3522
反应条件
n-Bu4NBrCl2
T=0°C; 0.0833333 h;
参考文献
Negoro; Ikeda
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 8 p. 2111 - 2115
反应条件
tetrabutylammomium bromide; chlorine in chloroform
T=15°C; 0.166667 h; Product distribution;
参考文献
Negoro; Ikeda
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 8 p. 2111 - 2115
参考文献
Urion; Namias
Bulletin de la Societe Chimique de France, 1936 , vol. <5> 3, p. 2333,2334