1-(环己基氨基)环己烷甲腈合成路线 (共 7 条)
反应条件
sodium hydrogen sulphate in water
1 h;
参考文献
Troyanskii, E. A.; Ioffe, V. A.; Mizintsev, V. V.; Nikishin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 1661 - 1667
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 8 p. 1814 - 1822
反应条件
benzeneseleninic anhydride in dichloromethane
T=20°C; 48 h;
参考文献
Barton, Derek H. R.; Billion, Annick; Boivin, Jean
Tetrahedron Letters, 1985 , vol. 26, # 9 p. 1229 - 1232
反应条件
1: 90 percent / HCl conc. / 24 h / 20 °C
2: 60 percent / NaHSO4 / H2O / 1 h
View Scheme
参考文献
Troyanskii, E. A.; Ioffe, V. A.; Mizintsev, V. V.; Nikishin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 1661 - 1667
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 8 p. 1814 - 1822
反应条件
1: 90 percent / HCl conc. / 24 h / 20 °C
2: 60 percent / NaHSO4 / H2O / 1 h
View Scheme
参考文献
Troyanskii, E. A.; Ioffe, V. A.; Mizintsev, V. V.; Nikishin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 1661 - 1667
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 8 p. 1814 - 1822
反应条件
sodium peroxodisulphate in water
T=70°C; 4.5 h; Product distribution;
参考文献
Troyanskii, E. A.; Ioffe, V. A.; Mizintsev, V. V.; Nikishin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 1661 - 1667
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 8 p. 1814 - 1822
反应条件
sodium hydroxide; sodium peroxodisulphate in water
T=70°C; 4.5 h; Product distribution;
参考文献
Troyanskii, E. A.; Ioffe, V. A.; Mizintsev, V. V.; Nikishin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 1661 - 1667
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 8 p. 1814 - 1822
参考文献
Koetz; Merkel
Journal fuer Praktische Chemie (Leipzig), 1926 , vol. <2> 113, p. 74