2-[(1-苯基乙基)氨基]乙醇合成路线 (共 10 条)
参考文献
Uhan Corporation
Patent: US5990311 A1, 1999 ;
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 64 h;
参考文献
Horwell, David C.; Lewthwaite, Russell A.; Pritchard, Martyn C.; Ratcliffe, Giles S.; Rubin, J. Ronald
Tetrahedron, 1998 , vol. 54, # 18 p. 4591 - 4606
反应条件
in dimethyl sulfoxide T=50°C; 72 h;
参考文献
Couty, Francois; Evano, Gwilherm; Vargas-Sanchez, Monica; Bouzas, Gloria
Journal of Organic Chemistry, 2005 , vol. 70, # 22 p. 9028 - 9031
参考文献
Nelson, Todd D.; Rosen, Jonathan D.; Brands, Karel M.J.; Craig, Bridgette; Huffman, Mark A.; McNamara, James M.
Tetrahedron Letters, 2004 , vol. 45, # 48 p. 8917 - 8920
反应条件
in water 0.333333 h; Sonication;
参考文献
Aparicio, David M.; Teran, Joel L.; Roa, Luis F.; Gnecco, Dino; Juarez, Jorge R.; Orea, Maria L.; Mendoza, Angel; Flores-Alamo, Marcos; Micouin, Laurent
Synthesis, 2011 , # 14 art. no. M11511SS, p. 2310 - 2320
反应条件
1: 100 percent / pyridine / CH2Cl2 / 0.5 h / 0 °C 2: 81 percent / LAH / tetrahydrofuran / 64 h View Scheme
参考文献
Tetrahedron, , vol. 54, # 18 p. 4591 - 4606
参考文献
Journal of Medicinal Chemistry, , vol. 44, # 16 p. 2555 - 2564
反应条件
1: 74 percent / NaHCO3; NaI / dimethylformamide / 7 h / 20 °C 2: SOCl2 / CH2Cl2 / 2 h / Heating 3: 380 mg / LiHMDS / tetrahydrofuran / 2 h / -78 - 20 °C View Scheme
参考文献
Couty, Francois; Evano, Gwilherm; Vargas-Sanchez, Monica; Bouzas, Gloria
Journal of Organic Chemistry, 2005 , vol. 70, # 22 p. 9028 - 9031
反应条件
sodium periodate in methanol; water 4 h; Ambient temperature;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 33, # 7 p. 692 - 693
反应条件
thionyl bromide in benzene 3 h; water bath;
参考文献
Potapov, V. M.; Dem'yanovich, V. M.; Skvortsova, T. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 9 p. 990 - 992
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 9 p. 1238 - 1240