3-羟基-1,3,3-三苯基-丙-1-酮合成路线 (共 23 条)
反应条件
1: 1.) Mg / 1.) ether 2.) ether, reflux
2: 70 percent / HgO, BF3*(C2H5)2O / H2O; tetrahydrofuran / Ambient temperature
View Scheme
参考文献
Stahl, Ingfried; Gosselck, Juergen
Synthesis, 1980 , # 7 p. 561 - 563
反应条件
hydrogenchloride; n-butyllithium; acetic acid
1) -78 deg C, 2 h, THF, hexane, 2) H2O, methanol, room temperature, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Matsumura, Noboru; Kunugihara, Akira; Yoneda, Shigeo
Tetrahedron Letters, 1983 , vol. 24, # 31 p. 3239 - 3242
参考文献
Erickson; Stansbury
Pr.Louisiana Acad., 1942 , vol. 6, p. 89,91
参考文献
Castelli,F.; Cannone,P.
Bulletin de la Societe Chimique de France, 1974 , p. 317 - 330
反应条件
oxygen in dichloromethane
T=25°C; 24 h; other reagents; Product distributionMechanism;
参考文献
Yamamoto, Hiroshi; Miura, Masahiro; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 173 - 182
参考文献
Vorlaender; Osterburg; Meye
Chemische Berichte, 1923 , vol. 56, p. 1143
参考文献
Dilthey; Last
Chemische Berichte, 1904 , vol. 37, p. 2640,3775
参考文献
Vorlaender; Osterburg; Meye
Chemische Berichte, 1923 , vol. 56, p. 1143
反应条件
hydrogenchloride; acetic acid
参考文献
Vorlaender; Osterburg; Meye
Chemische Berichte, 1923 , vol. 56, p. 1143
参考文献
Vorlaender; Osterburg; Meye
Chemische Berichte, 1923 , vol. 56, p. 1143