2,2,2-三甲基乙酰苯胺合成路线 （共 72 条）
反应条件
tris(N-2',6'-diisopropylphenyl(naphthyl)amidate)yttrium mono(tetrahydrofurane) in toluene T=20°C; 0.0833333 h; Inert atmosphere;
参考文献
Thomson, Jaclyn A.; Schafer, Laurel L.
Dalton Transactions, 2012 , vol. 41, # 26 p. 7897 - 7904
参考文献
Journal of the American Chemical Society, , vol. 53, p. 1065
Journal of the American Chemical Society, , vol. 56, p. 2117,2119
Journal of the American Chemical Society, , vol. 60, p. 2267
反应条件
1.1: 84 percent / NEt3 / CH2Cl2 / 2 h / 20 °C 2.1: tetrahydrofuran / -78 - 0 °C 2.2: 78 percent / H2O / tetrahydrofuran View Scheme
参考文献
Chemical Communications, , # 7 p. 933 - 935
反应条件
1.1: 84 percent / NEt3 / CH2Cl2 / 2 h / 20 °C 2.1: tetrahydrofuran / -78 - 0 °C 2.2: 78 percent / H2O / tetrahydrofuran View Scheme
参考文献
Chemical Communications, , # 7 p. 933 - 935
反应条件
1.1: 56 percent / K2CO3 / acetonitrile / 24 h / Heating 2.1: 84 percent / NEt3 / CH2Cl2 / 2 h / 20 °C 3.1: tetrahydrofuran / -78 - 0 °C 3.2: 78 percent / H2O / tetrahydrofuran View Scheme
参考文献
Chemical Communications, , # 7 p. 933 - 935
反应条件
1: DCC-DMAP 2: 66 percent / FeCl3 / CH2Cl2 / 13 h / Ambient temperature View Scheme
参考文献
Chemistry Letters, , p. 701 - 704
反应条件
1: Pd(OAc)2 / acetonitrile / 0.5 h / 6619.6 Torr / Ambient temperature 2: acetonitrile / 2 h / Ambient temperature; other educts View Scheme
参考文献
Journal of Organic Chemistry, , vol. 46, p. 4413 - 4416
反应条件
sodium carbonate in dichloromethane; water T=80°C;
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 18 p. 3373 - 3379
反应条件
in tetrahydrofuran 1.) 0 deg C, 1 h, 2.) r.t., overnight;
参考文献
Smith, Keith; El-Hiti, Gamal A.; Hamilton, Anna
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 24 p. 4041 - 4042
反应条件
bromo-dimethylsulfonium bromide T=80°C; Beckmann rearrangement; 2 h; Ionic liquid;
参考文献
Tetrahedron Letters, , vol. 51, # 4 p. 739 - 743
