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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
邻溴苯甲醛
合成路线
（共 635 条）
6630-33-7
邻溴苯甲醛
→
反应条件
61607-84-9
反应条件
tetrachloromethane; nickel; copper in N,N-dimethyl-formamide T=60°C; Chlorination; 5 h;
参考文献
Leonel, Eric; Paugam, Jean-Paul; Heintz, Monique; Nedelec, Jean-Yves
Synthetic Communications, 1999 , vol. 29, # 22 p. 4015 - 4024
6630-33-7
邻溴苯甲醛
→
反应条件
61608-94-4
反应条件
1: sodium tetrahydroborate / dichloromethane / 20 °C 2: anhydrous iron chloride / 10 h / 100 °C 3: diisopropylamine; bis(benzonitrile)palladium(II) dichloride; copper(l) iodide / toluene / 10 h / 110 °C 4: potassium carbonate / methanol / 20 °C 5: (p-CF3-C6H4)3P-Au-NTf2 / 1,2-dichloro-ethane / 10 h / 80 °C View Scheme
参考文献
Shu, Chao; Chen, Cheng-Bin; Chen, Wei-Xi; Ye, Long-Wu
Organic Letters, 2013 , vol. 15, # 21 p. 5542 - 5545
6630-33-7
邻溴苯甲醛
→
反应条件
1961-96-2
1-苯基茚; 1-苯基-1H-茚
+
61608-94-4
反应条件
1: sodium tetrahydroborate / dichloromethane / 20 °C 2: anhydrous iron chloride / 10 h / 100 °C 3: diisopropylamine; bis(benzonitrile)palladium(II) dichloride; copper(l) iodide / toluene / 10 h / 110 °C 4: potassium carbonate / methanol / 20 °C 5: 2-(dicyclohexylphosphino)-2',4',6'-triisopropylbiphenyl Au bis(trifluoromethylsulfonyl)imide / 1,2-dichloro-ethane / 10 h / 80 °C View Scheme
参考文献
Shu, Chao; Chen, Cheng-Bin; Chen, Wei-Xi; Ye, Long-Wu
Organic Letters, 2013 , vol. 15, # 21 p. 5542 - 5545
3054-95-3
丙烯醛缩二乙醇
+
6630-33-7
邻溴苯甲醛
→
反应条件
61650-52-0
反应条件
1: With potassium chloride; tetra-n-butylammonium acetate; palladium diacetate; potassium carbonate in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere; 2: With hydrogenchloride; water in N,N-dimethyl-formamide T=20°C; 0.25 h;
参考文献
Akagawa, Kengo; Sakamoto, Seiji; Kudo, Kazuaki
Synlett, 2011 , # 6 p. 817 - 820
6630-33-7
邻溴苯甲醛
→
反应条件
61650-52-0
反应条件
1: n-Bu4NOAc; K2CO3; KCl / Pd(OAc)2 / dimethylformamide / 3 h / 90 °C 2: aq. HCl / dimethylformamide / 0.17 h / 20 °C View Scheme
参考文献
Battistuzzi, Gianfranco; Cacchi, Sandro; Fabrizi, Giancarlo
Organic Letters, 2003 , vol. 5, # 5 p. 777 - 780
78-40-0
磷酸三乙酯(TEP)
+
74497-02-2
+
6630-33-7
邻溴苯甲醛
→
反应条件
61700-92-3
反应条件
phosphotungstic acid supported on imidazole functionalized silica coated cobalt ferrite nanoparticle in neat (no solvent) T=20°C; 0.5 h;
参考文献
Hamadi; Kooti; Afshari; Ghiasifar; Adibpour
Journal of Molecular Catalysis A: Chemical, 2013 , vol. 373, p. 25 - 29
74497-02-2
+
762-04-9
亚磷酸二乙酯
+
6630-33-7
邻溴苯甲醛
→
反应条件
61700-92-3
反应条件
Cp2Zr(OSO2C4H9)2*2H2O in neat (no solvent) T=20°C; Kabachnik-Fields Reaction; 3 h;
参考文献
Li, Ningbo; Wang, Xie; Qiu, Renhua; Xu, Xinhua; Chen, Jinyang; Zhang, Xiaohong; Chen, Sihai; Yin, Shuangfeng
Catalysis Communications, 2014 , vol. 43, p. 184 - 187
6630-33-7
邻溴苯甲醛
→
反应条件
61765-22-8
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / -78 - 20 °C / Inert atmosphere 2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere 2.2: Inert atmosphere 3.1: pyridinium chlorochromate / dichloromethane / 4 h / 20 °C / Inert atmosphere 4.1: potassium hydrogen persulfate; 18-crown-6 ether; sodium hydrogencarbonate; acetone / water; acetonitrile / 0 °C / Inert atmosphere 5.1: benzene / UV-irradiation; Inert atmosphere View Scheme
参考文献
Shao, Yutian; Yang, Chao; Gui, Weijun; Liu, Yang; Xia, Wujiong
Chemical Communications, 2012 , vol. 48, # 29 p. 3560 - 3562
6630-33-7
邻溴苯甲醛
→
反应条件
61981-67-7
反应条件
1: methanol / 12 h / -30 °C / |Reflux 2: potassium phosphate; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; bis(dibenzylideneacetone)-palladium(0) / toluene / 12 h / |Inert atmosphere; |Reflux 3: toluene / 24 h / |Reflux 4: potassium phosphate / 1,4-dioxane / 3 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Guan, Zong; Wiechmann, Sascha; Drafz, Martin; Huebner, Eike; Schmidt, Andreas
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 21 p. 3558 - 3567
6630-33-7
邻溴苯甲醛
→
反应条件
62403-86-5
1-(2-溴苯基)丙烷-1-酮
反应条件
1: tetrahydrofuran / 3.5 h / -78 - 25 °C 2: H2CrO4 / diethyl ether / 3 h / 25 °C View Scheme
参考文献
Matsuda, Takanori; Shigeno, Masanori; Makino, Masaomi; Murakami, Masahiro
Organic Letters, 2006 , vol. 8, # 15 p. 3379 - 3381
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