2-[(2,5-二甲基苯基)磺酰基]-1,4-二甲基苯合成路线 （共 9 条）
反应条件
Fe(3+)-montmorillonite
T=138°C; Substitution; Friedel-Crafts sulfonation; 24 h;
参考文献
Choudary, Boyapati M.; Chowdari, N. Sreenivasa; Kantam, M. Lakshmi
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 16 p. 2689 - 2693
反应条件
Benzoesaeure-fluorsulfonsaeureanhydrid in dichloromethane
T=0°C; 14 h; Title compound not separated from byproducts;
参考文献
Effenberger, Franz; Huthmacher, Klaus; Keil, Michael
Chemische Berichte, 1981 , vol. 114, # 5 p. 1967 - 1971
反应条件
SbF5; epoxysulfonyl fluoride
T=25°C; 1 h; Yield given. Yields of byproduct given;
参考文献
Tanaka, Mutsuo; Souma, Yoshie
Journal of Organic Chemistry, 1992 , vol. 57, # 13 p. 3738 - 3740
反应条件
1: SOCl2, AlCl3 / CS2 / 20 °C
2: 35percent H2O2, acetic acid / Heating
View Scheme
参考文献
Bulgarevich, S. B.; Movshovich, D. Ya.; Ivanova, N. A.; Filippov, S. E.; Finocchiaro, P.; Failla, S.
Russian Journal of General Chemistry, 1993 , vol. 63, # 3.1 p. 379 - 387
Zhurnal Obshchei Khimii, 1993 , vol. 63, # 3 p. 541 - 553
反应条件
in dichloromethane
T=0°C; 14 h; Title compound not separated from byproducts;
参考文献
Effenberger, Franz; Huthmacher, Klaus; Keil, Michael
Chemische Berichte, 1981 , vol. 114, # 5 p. 1967 - 1971
反应条件
dihydrogen peroxide; acetic acid
Heating; Yield given;
参考文献
Bulgarevich, S. B.; Movshovich, D. Ya.; Ivanova, N. A.; Filippov, S. E.; Finocchiaro, P.; Failla, S.
Russian Journal of General Chemistry, 1993 , vol. 63, # 3.1 p. 379 - 387
Zhurnal Obshchei Khimii, 1993 , vol. 63, # 3 p. 541 - 553
参考文献
Pollak et al.
Monatshefte fuer Chemie, 1930 , vol. 55, p. 358,373
参考文献
Gilbert et al.
Industrial and Engineering Chemistry, 1953 , vol. 45, p. 2065,2066
参考文献
Toehl; Eberhard
Chemische Berichte, 1893 , vol. 26, p. 2942
