3-(环己基氨基)丙酸乙酯合成路线 （共 6 条）
反应条件
potassium carbonate; tetra-(n-butyl)ammonium iodide
T=80°C; Neat (no solvent);
参考文献
Player, Mark R.; Huang, Hui; Hutta, Daniel A.
Patent: US2007/60577 A1, 2007 ;
Location in patent: Page/Page column 39 ;
US 20070060577 A1
反应条件
sodium tris(acetoxy)borohydride in methanol; dichloromethane
T=20°C; 6 h;
参考文献
Yen, Chi-Feng; Hu, Cheng-Kung; Chou, Ming-Chen; Tseng, Chen-Tso; Wu, Chien-Huang; Huang, Ying-Huey; Chen, Shu-Jen; King, Chi-Hsin Richard
Patent: US2006/281712 A1, 2006 ;
Location in patent: Page/Page column 105-106 ;
US 20060281712 A1
反应条件
in ethanol
2 h; Heating / reflux;
参考文献
Shiseido Company, Limited
Patent: EP1941861 A1, 2008 ;
Location in patent: Page/Page column 20-21 ;
反应条件
bromo-dimethylsulfonium bromide
T=20°C; Michael addition; 0.166667 h;
参考文献
Khan, Abu T.; Parvin, Tasneem; Gazi, Sarifuddin; Choudhury, Lokman H.
Tetrahedron Letters, 2007 , vol. 48, # 22 p. 3805 - 3808
反应条件
1: hydroquinone / 200 °C
2: hydrogen chloride; ethanol
View Scheme
参考文献
Hromatka; Eiles
Monatshefte fuer Chemie, 1948 , vol. 78, p. 129,135
反应条件
1: unter Entfernen des entstehenden Wassers
2: hydroquinone / 200 °C
3: hydrogen chloride; ethanol
View Scheme
参考文献
Hromatka; Eiles
Monatshefte fuer Chemie, 1948 , vol. 78, p. 129,135
