1-(三甲基硅氧烷)环己烯合成路线 (共 370 条)
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane T=40°C; 1 h;
参考文献
Lin, Ji-Mao; Liu, Ben-Sheng
Synthetic Communications, 1997 , vol. 27, # 5 p. 739 - 749
反应条件
(dimethylamino)trimethylsilane in dichloromethane 1.) 30 min, -30 deg C; 2.) 15 h, 20 deg C;
参考文献
Schroth, Werner; Jahn, Ullrich; Stroehl, Dieter
Chemische Berichte, 1994 , vol. 127, # 10 p. 2013 - 2022
反应条件
sodium hydride in diethyl ether; Petroleum ether 5 h;
参考文献
Hurdlik, Paul F.; Hudrlik, Anne M.; Kulkarni Ashok K.
Journal of the American Chemical Society, 1985 , vol. 107, # 14 p. 4260 - 4264
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; 1 h;
参考文献
Kita, Yasuyuki; Yasuda, Hitoshi; Haruta, Jun-ichi; Segawa, Jun; Tamura, Yasumitsu
Synthesis, 1982 , # 12 p. 1089 - 1091
反应条件
SmI3(tetrahydrofuran)3 in dichloromethane 0.166667 h; Ambient temperature;
参考文献
Giuseppone, Nicolas; Van De Weghe, Pierre V.; Mellah, Mohamed; Collin, Jacqueline
Tetrahedron, 1998 , vol. 54, # 43 p. 13129 - 13148
反应条件
diisopropylamine; lithium chloride in tetrahydrofuran T=0°C; 18 h;
参考文献
Synlett, , # 9 p. 1386 - 1390
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
参考文献
Journal of the American Chemical Society, , vol. 98, p. 2346 - 2348
反应条件
1,1,1,3,3,3-hexamethyl-disilazane; sodium iodide in tetrahydrofuran; dichloromethane T=0°C;
参考文献
Journal of Organic Chemistry, , vol. 52, # 17 p. 3919 - 3920
反应条件
C9H12BNO*C2HF6NO4S2 in dichloromethane T=-78°C; 0.5 h; Inert atmosphere;
参考文献
Kang, Byung Chul; Shim, Su Yong; Ryu, Do Hyun
Organic Letters, 2014 , vol. 16, # 8 p. 2077 - 2079
反应条件
hydrido(triphenylphosphine)copper(I) hexamer in benzene-d6 Ambient temperature;
参考文献
Mahoney, Wayne S.; Brestensky, Donna M.; Sryker, Jeffrey M.
Journal of the American Chemical Society, 1988 , vol. 110, # 1 p. 291 - 293