1-(三甲基硅氧烷)环己烯合成路线 (共 370 条)
反应条件
in dichloromethane T=20°C;
参考文献
Rudler, Henri; Parlier, Andree; Denneval, Charline; Herson, Patrick
Journal of Fluorine Chemistry, 2010 , vol. 131, # 6 p. 738 - 741
反应条件
1: With dimethylsulfide borane complex in tetrahydrofuran T=0 - 20°C; 2: With benzene-1,2-diol; triethylamine in tetrahydrofuran T=0 - 20°C; 3: With oxygen in tetrahydrofuran T=20°C; 12 h; Further stages.;
参考文献
Cadot, Christine; Dalko, Peter I.; Cossy, Janine; Ollivier, Cyril; Chuard, Rachel; Renaud, Philippe
Journal of Organic Chemistry, 2002 , vol. 67, # 21 p. 7193 - 7202
反应条件
hydrogenchloride in dichloromethane
参考文献
Allied-Signal Inc.
Patent: US5254732 A1, 1993 ;
反应条件
XeF2 in acetonitrile T=20°C; 1 h;
参考文献
Ramsden, Christopher A.; Smith, Rachel G.
Organic Letters, 1999 , vol. 1, # 10 p. 1591 - 1594
反应条件
fluorine in various solvent(s) T=-78°C; 3.5 h;
参考文献
Purrington, Suzane T.; Lazaridis, Nicholas V.; Bumgardner, Carl L.
Tetrahedron Letters, 1986 , vol. 27, # 24 p. 2715 - 2716
参考文献
Allied-Signal Inc.
Patent: US5086190 A1, 1992 ;
反应条件
XeF2 in dichloromethane var. solv. and material of vessel; Mechanism;
参考文献
Ramsden; Smith
Journal of the American Chemical Society, 1998 , vol. 120, # 27 p. 6842 - 6843
反应条件
chloromethyl methyl ether; tin(ll) chloride in dichloromethane 1 h; Ambient temperature;
参考文献
Oriyama, Takeshi; Iwanami, Katsuyuki; Miyauchi,Yuka; Koga, Gen
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 12 p. 3716 - 3718
反应条件
acetyl chloride; tin(ll) chloride in dichloromethane 2 h; Ambient temperatureeffect of catalyst-activator system; Product distribution;
参考文献
Oriyama, Takeshi; Iwanami, Katsuyuki; Miyauchi,Yuka; Koga, Gen
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 12 p. 3716 - 3718
反应条件
{[γ-SiW10O32(H2O)2]2(μ-O)2}4- in nitromethane T=31.84°C; Mukaiyama aldol reaction;
参考文献
Journal of Organometallic Chemistry, , vol. 692, # 1-3 p. 455 - 459