1-(三甲基硅氧烷)环己烯合成路线 （共 370 条）
反应条件
(CF3CH2O)VOCl2 T=-78°C; 0.5 h;
参考文献
Fujii Takashi; Hirao, Toshikazu; Ohshiro, Yoshiki
Tetrahedron Letters, 1992 , vol. 33, # 39 p. 5823 - 5826
反应条件
[VO(OEt)Cl2] in dichloromethane 1) -75 deg C, 3 h, 2) -30 deg C, 4 h;
参考文献
Fujii Takashi; Hirao, Toshikazu; Ohshiro, Yoshiki
Tetrahedron Letters, 1992 , vol. 33, # 39 p. 5823 - 5826
反应条件
1: tris-(dibenzylideneacetone)dipalladium(0); tri-n-butyltin fluoride; triethylamine; [(t-Bu)3PH]BF4 / benzene / 24 h / 80 °C / Inert atmosphere 2: pyridine; sodium iodide / hexane; acetonitrile / 20 h / 20 °C 3: (R)-N-(5,5,4,4,3,3,2,2-octafluoropentyl)-tert-butanesulfinamide; 2,6-di-tert-butyl-phenol; 2,4-Dinitrobenzenesulfonic acid; sodium sulfate / toluene / -78 - -50 °C View Scheme
参考文献
Beck, Elizabeth M.; Hyde, Alan M.; Jacobsen, Eric N.
Organic Letters, 2011 , vol. 13, # 16 p. 4260 - 4263
反应条件
chloromethyl methyl ether; tin(ll) chloride in dichloromethane 1 h; Ambient temperature;
参考文献
Oriyama, Takeshi; Iwanami, Katsuyuki; Miyauchi,Yuka; Koga, Gen
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 12 p. 3716 - 3718
反应条件
acetyl chloride; tin(ll) chloride in dichloromethane 2 h; Ambient temperatureeffect of catalyst-activator system; Product distribution;
参考文献
Oriyama, Takeshi; Iwanami, Katsuyuki; Miyauchi,Yuka; Koga, Gen
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 12 p. 3716 - 3718
反应条件
{[γ-SiW10O32(H2O)2]2(μ-O)2}4- in nitromethane T=31.84°C; Mukaiyama aldol reaction;
参考文献
Yoshida, Akihiro; Hikichi, Shiro; Mizuno, Noritaka
Journal of Organometallic Chemistry, 2007 , vol. 692, # 1-3 p. 455 - 459
反应条件
antimony trichloride in dichloromethane T=0°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 47, # 26 p. 5099 - 5102
反应条件
tri-tert-butyl phosphine; tri-n-butyltin fluoride; tris(dibenzylideneacetone)dipalladium (0) in benzene 21 h; Heating;
参考文献
Iwama, Tetsuo; Rawal, Viresh H.
Organic Letters, 2006 , vol. 8, # 25 p. 5725 - 5728
反应条件
bis (triortho-tolylphosphine)palladium(II) chloride; tri-n-butyltin fluoride in benzene 3 h; Heating;
参考文献
Kuwajima, Isao; Urabe, Hirokazu
Journal of the American Chemical Society, 1982 , vol. 104, # 24 p. 6831 - 6833
反应条件
in tetrahydrofuran -70 deg C to r.t.; Yield given;
参考文献
Chen, Kuanchiang; Koser, Gerald F.
Journal of Organic Chemistry, 1991 , vol. 56, # 20 p. 5764 - 5767
