1-(三甲基硅氧烷)环己烯合成路线 （共 370 条）
反应条件
in tetrahydrofuran 1) < -38 deg C, 2 h 50 min 2) to 10 deg C, 2 h 3) r.t., 30 min;
参考文献
Chen, Kuanchiang; Koser, Gerald F.
Journal of Organic Chemistry, 1991 , vol. 56, # 20 p. 5764 - 5767
反应条件
water; cesium fluoride 1.) 60 deg C, 11h; Yield given. Multistep reaction;
参考文献
Boyer, J.; Corriu, R. J. P.; Perz, R.; Reye, C.
Journal of Organometallic Chemistry, 1980 , vol. 184, # 2 p. 157 - 166
反应条件
trichlorophosphate 1.) CH2Cl2, 0-10 deg C, 30 min; 2.) room temp., 15 h; Yield given. Multistep reaction;
参考文献
Synthesis, , # 6 p. 575 - 577
反应条件
water; cesium fluoride 1.) 80 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Boyer, J.; Corriu, R. J. P.; Perz, R.; Reye, C.
Journal of Organometallic Chemistry, 1980 , vol. 184, # 2 p. 157 - 166
反应条件
zinc(II) iodide in 1,4-dioxane
参考文献
Kubota, Toshio; Iijima, Masahiro; Tanaka, Tatsuo
Tetrahedron Letters, 1992 , vol. 33, # 10 p. 1351 - 1354
反应条件
hydrogenchloride in tetrahydrofuran 0.5 h; Ambient temperature; Yield given;
参考文献
Kita, Yasuyuki; Yasuda, Hitoshi; Haruta, Jun-ichi; Segawa, Jun; Tamura, Yasumitsu
Synthesis, 1982 , # 12 p. 1089 - 1091
反应条件
hydrogenchloride in tetrahydrofuran 0.5 h; Ambient temperature; Yield given;
参考文献
Kita, Yasuyuki; Yasuda, Hitoshi; Haruta, Jun-ichi; Segawa, Jun; Tamura, Yasumitsu
Synthesis, 1982 , # 12 p. 1089 - 1091
反应条件
titanium tetrachloride in dichloromethane T=-78°C; 2 h;
参考文献
House, Herbert O.; Outcalt, Russell J.; Cliffton, Michael D.
Journal of Organic Chemistry, 1982 , vol. 47, # 12 p. 2413 - 2419
反应条件
titanium tetrachloride in dichloromethane T=-40°C; 1 h;
参考文献
Reetz, Manfred T.; Maier, Wilhelm F.; Chatziiosifidis, Ioannis; Giannis, Athanassios; Heimbach, Horst; Loewe, Ursula
Chemische Berichte, 1980 , vol. 113, # 12 p. 3741 - 3757
反应条件
aluminum oxide; zinc(II) chloride T=-10°C; Alkylation; 1.5 h;
参考文献
Kad; Singh, Vasundhara; Khurana, Anupam; Chaudhary, Sangeeta; Singh, Jasvinder
Synthetic Communications, 1999 , vol. 29, # 19 p. 3439 - 3442
