1-(三甲基硅氧烷)环己烯合成路线 (共 370 条)
反应条件
potassium cyanide; 18-crown-6 ether in tetrahydrofuran 24 h; Ambient temperature;
参考文献
Gostevskii, B. A.; Kruglaya, O. A.; Albanov, A. I.; Vyazankin, N. S.
Journal of Organometallic Chemistry, 1980 , vol. 187, # 2 p. 157 - 166
反应条件
trifluorormethanesulfonic acid T=15°C; 0.25 h;
参考文献
Aizpurua, Jesus M.; Palomo, Claudio; Palomo, Antonio L.
Canadian Journal of Chemistry, 1984 , vol. 62, p. 336 - 340
反应条件
tetrabutylammomium bromide T=105°C; 4 h; Product distribution; Further Variations:ReagentsTemperatures;
参考文献
Smietana, Michael; Mioskowski, Charles
Organic Letters, 2001 , vol. 3, # 7 p. 1037 - 1039
反应条件
palladium dichloride; phosphorous acid trimethyl ester in benzene T=80°C; 5 h;
参考文献
Kosugi, Masanori; Ohya, Takao; Migita, Toshihiko
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 11 p. 3539 - 3540
反应条件
(trimethylsilyl)manganese pentacarbonyl T=50°C; 2 h; other α-bromo carbonyl compounds; var. temp. and times; Product distributionMechanism;
参考文献
Marsi, Marianne; Brinkman, Kerry C.; Lisensky, Carol A.; Vaughn, George D.; Gladysz, J. A.
Journal of Organic Chemistry, 1985 , vol. 50, # 18 p. 3396 - 3401
反应条件
pyridine; chromium(VI) oxide in dichloromethane T=20°C; 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1934 - 1941
反应条件
trifluorormethanesulfonic acid in dichloromethane 0.333333 h; ice cooling to r.t.; other ketones;
参考文献
Olah, George A.; Husain, Altaf; Gupta, B. C. Balaram; Salem, George F.; Narang, Subhash C.
Journal of Organic Chemistry, 1981 , vol. 46, p. 5212 - 5214
反应条件
tetraphenyl stibonium bromide; N-phenyl-2-methylazilidine in dichloromethane T=40°C; 3 h; Mechanism;
参考文献
Chemistry Letters, , p. 1247 - 1250
反应条件
1: 30 percent / bis<benzyltriethylammonium> dichromate / hexamethylphosphoric acid triamide / 60 - 80 °C 2: 70 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1 h / 20 °C View Scheme
参考文献
Synthesis, , # 12 p. 1089 - 1091
反应条件
trimethylsilyl trifluoromethanesulfonate T=-30°C;
参考文献
Tetrahedron Letters, , vol. 34, # 37 p. 5863 - 5866