1-(三甲基硅氧烷)环己烯合成路线 （共 370 条）
反应条件
zinc(II) chloride in dichloromethane T=22°C; 48 h; SnCl4;
参考文献
Reetz, Manfred T.; Maier, Wilhelm F.; Heimbach, Horst; Giannis, Athanassios; Anastassious, Georgia
Chemische Berichte, 1980 , vol. 113, # 12 p. 3734 - 3740
反应条件
zinc(II) chloride in dichloromethane T=60°C; 8 h;
参考文献
Reetz, Manfred T.; Maier, Wilhelm F.; Heimbach, Horst; Giannis, Athanassios; Anastassious, Georgia
Chemische Berichte, 1980 , vol. 113, # 12 p. 3734 - 3740
反应条件
titanium tetrachloride in dichloromethane T=-40°C; 4 h; var. temp., time; Product distribution;
参考文献
Reetz, Manfred T.; Maier, Wilhelm F.; Heimbach, Horst; Giannis, Athanassios; Anastassious, Georgia
Chemische Berichte, 1980 , vol. 113, # 12 p. 3734 - 3740
反应条件
tri-tert-butyl phosphine; tri-n-butyltin fluoride; tris(dibenzylideneacetone)dipalladium (0) in benzene 20 h; Heating;
参考文献
Iwama, Tetsuo; Rawal, Viresh H.
Organic Letters, 2006 , vol. 8, # 25 p. 5725 - 5728
反应条件
silver trifluoroacetate in dichloromethane T=25°C; 0.166667 h;
参考文献
Jefford, Charles W.; Sledeski, Adam W.; Lelandais, Patrick; Boukouvalas, John
Tetrahedron Letters, 1992 , vol. 33, # 14 p. 1855 - 1858
反应条件
sodium tris(acetoxy)borohydride; acetic acid in 1,2-dichloro-ethane T=20°C; 2 h;
参考文献
Reddy, T. Jagadeeswar; Leclair, Michael; Proulx, Melanie
Synlett, 2005 , # 4 art. no. S07004ST, p. 583 - 586
反应条件
sodium tetrahydroborate; boron trifluoride diethyl etherate 1.) benzene, 25 deg C, 2 h, 2.) benzene, ethanol, from 0 deg C to 25 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Cheng, Yea-Shun; Ho, Eugene; Mariano, Patrick S.; Ammon, Herman L.
Journal of Organic Chemistry, 1985 , vol. 50, # 26 p. 5678 - 5686
反应条件
18-crown-6 ether; (RO)2P(O)SCl 1.) CH2Cl2, RT, 2.) DME, RT, 2 h; Yield given. Multistep reaction;
参考文献
Dybowski, Piotr; Skowronska, Aleksandra
Synthesis, 1997 , # 3 p. 284 - 286
反应条件
1: 79 percent / ZnBr2 View Scheme
参考文献
Ager, David J.
Tetrahedron Letters, 1983 , vol. 24, # 4 p. 419 - 422
反应条件
titanium(IV) isopropylate; titanium tetrachloride in dichloromethane -90 deg C, 90 min;
参考文献
Mateos, A. Fernandez; Fuente Blanco, Jesus A. de la
Journal of Organic Chemistry, 1990 , vol. 55, # 4 p. 1349 - 1354
