1-(三甲基硅氧烷)环己烯合成路线 (共 370 条)
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide
参考文献
Journal of Organometallic Chemistry, , vol. 153, p. 137 - 151
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide
参考文献
Journal of Organometallic Chemistry, , vol. 153, p. 137 - 151
反应条件
1: (carbomethoxymethyl)trimethylsilane; potassium hexamethylsilazane in tetrahydrofuran T=0°C; 0.5 h; 2: cyclohexanone in tetrahydrofuran T=-78°C; 2 h; Further stages.;
参考文献
Journal of Organic Chemistry, , vol. 67, # 21 p. 7378 - 7388
反应条件
dicobalt octacarbonyl T=110°C; 6 h;
参考文献
Sisak, Attila
Synthetic Communications, 2006 , vol. 36, # 24 p. 3693 - 3702
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide Ambient temperature;
参考文献
Dedier, James; Gerval, Pierre; Frainnet, Emile
Journal of Organometallic Chemistry, 1980 , vol. 185, # 2 p. 183 - 198
反应条件
1: 92.4 percent / lithium aluminium hydride / diethyl ether / 0.17 h 2: chromium trioxide, pyridine / CH2Cl2 / 2 h / 20 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1934 - 1941
反应条件
1: 83 percent / 49percent peracetic acid, sodium acetate / CH2Cl2 / 0.5 h / 20 °C 2: 92.4 percent / lithium aluminium hydride / diethyl ether / 0.17 h 3: chromium trioxide, pyridine / CH2Cl2 / 2 h / 20 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1934 - 1941
反应条件
pyrrolidin-2-one; tetraethylammonium tetrafluoroborate 1.) DME, HMPA, RT, electrochemical reduction, 2.) DME, HMPA, -75 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Journal of Organometallic Chemistry, , vol. 493, # 1-2 p. 27 - 32
反应条件
sodium trimethyl-silanolate
参考文献
Chemische Berichte, , vol. 102, # 1 p. 14 - 22
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 48, # 8 p. 1738 - 1742,1587 - 1590