1-(三甲基硅氧烷)环己烯合成路线 （共 370 条）
反应条件
lithium perchlorate; sodium carbonate in acetonitrile
参考文献
Renaud, Roger N.; Stephens, Campbell J.; Brochu, Gaetan
Canadian Journal of Chemistry, 1984 , vol. 62, p. 565 - 569
反应条件
titanium tetrachloride in dichloromethane
1.) -23 deg C, 1.5 h, 2.) -23 deg C to r.t.;
参考文献
Braga, Antonio L.; Dornelles, Luciano; Silveira, Claudio C.; Wessjohann, Ludger A.
Synthesis, 1999 , # 4 p. 562 - 564
反应条件
zinc(II) chloride in ethyl acetate
18 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Makin, S. M.; Kruglikova, R. I.; Tagirov, T. K.; Kharitonova, O. V.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 6 p. 1075 - 1078
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 6 p. 1182 - 1185
反应条件
hydrogenchloride; bismuth(III) chloride; sodium iodide
1) CH2Cl2, r.t., 2) r.t., 1.5 h; Yield given. Multistep reaction;
参考文献
Roux, Christophe Le; Gaspard-Iloughmane, Hafida; Dubac, Jacques; Jaud, Joel; Vignaux, Pierre
Journal of Organic Chemistry, 1993 , vol. 58, # 7 p. 1835 - 1839
反应条件
1,2-bis-(diphenylphosphino)ethane; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in tetrahydrofuran
12 h; Heating;
参考文献
Tsuji, Jiro; Minami, Ichiro; Shimizu, Isao
Chemistry Letters, 1983 , p. 1325 - 1326
反应条件
aluminum oxide; zinc(II) chloride
T=-10°C; Alkylation; 1.5 h;
参考文献
Kad; Singh, Vasundhara; Khurana, Anupam; Chaudhary, Sangeeta; Singh, Jasvinder
Synthetic Communications, 1999 , vol. 29, # 19 p. 3439 - 3442
反应条件
[VO(OEt)Cl2] in dichloromethane
T=-75°C; 2 h;
参考文献
Hirao, Toshikazu; Fujii, Takashi; Ohshiro, Yoshiki
Tetrahedron, 1994 , vol. 50, # 34 p. 10207 - 10214
反应条件
tin(IV) chloride in dichloromethane
T=-40°C; 1.5 h;
参考文献
Nsunda, K. M.; Hevesi, L.
Tetrahedron Letters, 1984 , vol. 25, # 39 p. 4441 - 4444
反应条件
Multistep reaction.;
参考文献
Cassel, Johan A.; Leue, Stefanie; Gachkova, Natalie I.; Kann, Nina C.
Journal of Organic Chemistry, 2002 , vol. 67, # 26 p. 9460 - 9463
反应条件
triethylamine in acetonitrile
24 h; Heating;
参考文献
Vega, Juan A.; Alajarin, Ramon; Vaquero, Juan J.; Alvarez-Builla, Julio
Tetrahedron, 1998 , vol. 54, # 14 p. 3589 - 3606
