1-(三甲基硅氧烷)环己烯合成路线 （共 370 条）
反应条件
in dichloromethane
16 h; Ambient temperaturefurther conditions: irradiation;
参考文献
Rathore, Rajendra; Kochi, Jay K.
Journal of Organic Chemistry, 1996 , vol. 61, # 2 p. 627 - 639
反应条件
silver trifluoroacetate in dichloromethane
T=25°C; 0.166667 h;
参考文献
Jefford, Charles W.; Sledeski, Adam W.; Lelandais, Patrick; Boukouvalas, John
Tetrahedron Letters, 1992 , vol. 33, # 14 p. 1855 - 1858
反应条件
1: 19 percent / titanium tetrachloride / CH2Cl2 / 1 h / -20 °C
2: AIBN, Bu3SnH / benzene / 1 h / Heating
View Scheme
参考文献
Beckwith,A.L.; O'Shea,D.M.; Westwood,S.W.
Journal of the American Chemical Society, 1988 , vol. 110, p. 2565
反应条件
molecular sieve; BnNMe3(+)F(-) in ethylene glycol dimethyl ether
1.) room temperature, overnight, 2.) -78 deg C, 5 min, 3.) 0 deg C, 6 h;
参考文献
Kuwajima, Isao; Nakamura, Eiichi; Shimizu, Makoto
Journal of the American Chemical Society, 1982 , vol. 104, # 4 p. 1025 - 1030
反应条件
trimethylsilyl iodide in dichloromethane
T=-78°C; 0.0833333 h;
参考文献
Hosomi, Akira; Sakata, Yasuyuki; Sakurai, Hideki
Chemistry Letters, 1983 , p. 405 - 408
反应条件
trimethylsilyl trifluoromethanesulfonate in acetonitrile
T=-10°C; 0.0833333 h;
参考文献
Hosomi, Akira; Sakata, Yasuyuki; Sakurai, Hideki
Chemistry Letters, 1983 , p. 405 - 408
反应条件
trimethylsilyl iodide in dichloromethane
T=-78°C; 0.0833333 h;
参考文献
Hosomi, Akira; Sakata, Yasuyuki; Sakurai, Hideki
Chemistry Letters, 1983 , p. 405 - 408
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane
4 h; Ambient temperature;
参考文献
Hosomi, Akira; Sakata, Yasuyuki; Sakurai, Hideki
Chemistry Letters, 1983 , p. 405 - 408
反应条件
chloro-trimethyl-silane; sodium iodide in acetonitrile
4 h; Ambient temperature;
参考文献
Hosomi, Akira; Sakata, Yasuyuki; Sakurai, Hideki
Chemistry Letters, 1983 , p. 405 - 408
反应条件
trimethylsilyl iodide in dichloromethane
1.) r.t., 1 h; 2.) reflux, 1.5 h;
参考文献
Hosomi, Akira; Sakata, Yasuyuki; Sakurai, Hideki
Chemistry Letters, 1983 , p. 405 - 408
