1-(三甲基硅氧烷)环己烯合成路线 （共 370 条）
反应条件
[(CH3)2N](CH3)2N=C-C=N(CH3)2[N(CH3)2](2+)*2F(1-) in acetonitrile T=20°C; desilylation; 96 h;
参考文献
Chambers, Richard D.; Gray, William K.; Sandford, Graham; Vaughan, Julian F.S.
Journal of Fluorine Chemistry, 1999 , vol. 94, # 2 p. 213 - 215
反应条件
oxygen; silica gel; palladium in N,N-dimethyl acetamide T=67.9°C; 24 h; Yields of byproduct given;
参考文献
Baba, Toshide; Nakano, Kaichiro; Nishiyama, Satoru; Tsuruya, Shigeru; Masai, Mitsuo
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1990 , # 7 p. 1113 - 1119
反应条件
hydrogen; [RuCl(η2-H2)(dppe)2]OTf in 1,2-dichloro-ethane T=50°C; P=760 Torr; 48 h; Product distribution; Further Variations:Catalysts;
参考文献
Takei, Izuru; Nishibayashi, Yoshiaki; Ishii, Youichi; Mizobe, Yasushi; Uemura, Sakae; Hidai, Masanobu
Journal of Organometallic Chemistry, 2003 , vol. 679, # 1 p. 32 - 42
反应条件
tris(cetyl)pyridinium 12-tungstophosphate; dihydrogen peroxide in dichloromethane T=20°C; 9 h;
参考文献
Journal of Organic Chemistry, , vol. 62, # 21 p. 7174 - 7177
反应条件
molecular sieve; BnNMe3(+)F(-) in tetrahydrofuran 1.) room temperature, overnight, 2.) 0 deg C, 10 min, 3.) room temperature, ,24 h;
参考文献
Journal of the American Chemical Society, , vol. 104, # 4 p. 1025 - 1030
反应条件
antimony trichloride in dichloromethane T=0°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 47, # 26 p. 5099 - 5102
反应条件
[VO(OEt)Cl2] in dichloromethane T=-75°C; 2 h;
参考文献
Hirao, Toshikazu; Fujii, Takashi; Ohshiro, Yoshiki
Tetrahedron, 1994 , vol. 50, # 34 p. 10207 - 10214
反应条件
molecular sieve; BnNMe3(+)F(-) in ethylene glycol dimethyl ether 1.) room temperature, overnight, 2.) -78 deg C, 5 min, 3.) 0 deg C, 6 h;
参考文献
Journal of the American Chemical Society, , vol. 104, # 4 p. 1025 - 1030
反应条件
XeF2 in dichloromethane var. solv. and material of vessel; Mechanism;
参考文献
Ramsden; Smith
Journal of the American Chemical Society, 1998 , vol. 120, # 27 p. 6842 - 6843
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Garst, Michael E.; Arrhenius, Peter
Journal of Organic Chemistry, 1983 , vol. 48, # 1 p. 16 - 24
