1: S-phenyl-N,N-diethyl-sulfenamide With tin(IV) chloride in tetrachloromethane T=0°C; 0.5 h; 2: hex-3-yne in tetrachloromethane T=20°C; 5 h; Title compound not separated from byproducts;
参考文献
Martynov; Makhaeva; Amosova
Russian Journal of Organic Chemistry, 2006 , vol. 42, # 7 p. 954 - 958
1: S-phenyl-N,N-diethyl-sulfenamide With tin(IV) chloride in tetrachloromethane T=0°C; 0.5 h; 2: hex-3-yne in tetrachloromethane T=20°C; 5 h; 3: With potassium tert-butylate in tert-butyl alcohol 1 h; Heating; Title compound not separated from byproducts;
参考文献
Martynov; Makhaeva; Amosova
Russian Journal of Organic Chemistry, 2006 , vol. 42, # 7 p. 954 - 958
1: S-phenyl-N,N-diethyl-sulfenamide With tin(IV) chloride in dichloromethane T=0°C; 0.5 h; 2: phenylacetylene in tetrachloromethane T=20°C; 14 h; 3: With potassium tert-butylate in tert-butyl alcohol 13 h; Heating; Title compound not separated from byproducts;
参考文献
Martynov; Makhaeva; Amosova
Russian Journal of Organic Chemistry, 2006 , vol. 42, # 7 p. 954 - 958
